Phosphine oxide, (1-cyclohexen-1-ylmethyl)diphenyl-

Base Information

Chemical Name:Phosphine oxide, (1-cyclohexen-1-ylmethyl)diphenyl-
CAS No.:76002-40-9
Molecular Formula:C19H21OP
Molecular Weight:296.349
Hs Code.:
DSSTox Substance ID:DTXSID50472516
Nikkaji Number:J3.398.096E
Wikidata:Q82301486

Synonyms:Phosphine oxide, (1-cyclohexen-1-ylmethyl)diphenyl-;76002-40-9;DTXSID50472516

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphine oxide, (1-cyclohexen-1-ylmethyl)diphenyl-

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:296.133002287
Heavy Atom Count:21
Complexity:378

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC(=CC1)CP(=O)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of Phosphine oxide, (1-cyclohexen-1-ylmethyl)diphenyl-

There total 6 articles about Phosphine oxide, (1-cyclohexen-1-ylmethyl)diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 87512-43-4
1-(diphenylphosphinoylmethyl)cyclohexanol

: 76002-40-9
1-(diphenylphosphinoylmethyl)cyclohexene

Guidance literature:: With trifluoroacetic acid;
DOI:10.1016/S0040-4039(00)61923-8

Reference yield:

: 2129-89-7
diphenyl(methyl)phosphine oxide

: 76002-40-9
1-(diphenylphosphinoylmethyl)cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / BuLi / tetrahydrofuran / 1.) -78 deg C, 10 min, 2.) warm to room temperature

2: 91 percent / TFA / 1 h / Heating

With n-butyllithium; trifluoroacetic acid; In tetrahydrofuran;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 76002-40-9
1-(diphenylphosphinoylmethyl)cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / BuLi / tetrahydrofuran / 1.) -78 deg C, 10 min, 2.) warm to room temperature

2: 91 percent / TFA / 1 h / Heating

With n-butyllithium; trifluoroacetic acid; In tetrahydrofuran;