1-[(Diphenylphosphoryl)methyl]cyclohexane-1,2-diol

Base Information

Chemical Name:1-[(Diphenylphosphoryl)methyl]cyclohexane-1,2-diol
CAS No.:89358-81-6
Molecular Formula:C₁₉H₂₃O₃P
Molecular Weight:330.364
Hs Code.:
DSSTox Substance ID:DTXSID80527205

Synonyms:89358-81-6;1-[(Diphenylphosphoryl)methyl]cyclohexane-1,2-diol;DTXSID80527205

Suppliers and Price of 1-[(Diphenylphosphoryl)methyl]cyclohexane-1,2-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(Diphenylphosphoryl)methyl]cyclohexane-1,2-diol

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:330.13848159
Heavy Atom Count:23
Complexity:404

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC(C(C1)O)(CP(=O)(C2=CC=CC=C2)C3=CC=CC=C3)O

Technology Process of 1-[(Diphenylphosphoryl)methyl]cyclohexane-1,2-diol

There total 5 articles about 1-[(Diphenylphosphoryl)methyl]cyclohexane-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 87512-44-5
1-(diphenylphosphinoylmethyl)-7-oxabicyclo<4.1.0>heptane

: 86488-93-9
2-<(diphenylphosphinyl)methyl>cyclohexanone

: 89358-81-6
1-(Diphenyl-phosphinoylmethyl)-cyclohexane-1,2-diol

Guidance literature:: With trifluoroacetic acid; Ambient temperature;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 89358-81-6
1-(Diphenyl-phosphinoylmethyl)-cyclohexane-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BuLi, 3.) TFA

2: 91 percent / MCPBA

3: 50 percent / TFA / Ambient temperature

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;

Reference yield:

: 87512-43-4
1-(diphenylphosphinoylmethyl)cyclohexanol

: 89358-81-6
1-(Diphenyl-phosphinoylmethyl)-cyclohexane-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / TFA

2: 91 percent / MCPBA

3: 50 percent / TFA / Ambient temperature

With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;