2(1H)-Isoquinolinecarboxylic acid, 3-[[[(1R)-1-carboxy-2-(4-chlorophenyl)ethyl]amino]methyl]-3,4-dihydro-, 2-(1,1-dimethylethyl) ester, (3R)-

Base Information

Chemical Name:2(1H)-Isoquinolinecarboxylic acid, 3-[[[(1R)-1-carboxy-2-(4-chlorophenyl)ethyl]amino]methyl]-3,4-dihydro-, 2-(1,1-dimethylethyl) ester, (3R)-
CAS No.:760167-36-0
Molecular Formula:C24H29ClN2O4
Molecular Weight:444.958
Hs Code.:

2(1H)-Isoquinolinecarboxylic acid,
3-[[[(1R)-1-carboxy-2-(4-chlorophenyl)ethyl]amino]methyl]-3,4-dihydro-,
2-(1,1-dimethylethyl) ester, (3R)-

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Chemical Property of 2(1H)-Isoquinolinecarboxylic acid, 3-[[[(1R)-1-carboxy-2-(4-chlorophenyl)ethyl]amino]methyl]-3,4-dihydro-, 2-(1,1-dimethylethyl) ester, (3R)-

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Technology Process of 2(1H)-Isoquinolinecarboxylic acid, 3-[[[(1R)-1-carboxy-2-(4-chlorophenyl)ethyl]amino]methyl]-3,4-dihydro-, 2-(1,1-dimethylethyl) ester, (3R)-

There total 1 articles about 2(1H)-Isoquinolinecarboxylic acid, 3-[[[(1R)-1-carboxy-2-(4-chlorophenyl)ethyl]amino]methyl]-3,4-dihydro-, 2-(1,1-dimethylethyl) ester, (3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 444583-49-7
tert-butyl (3R)-3-({[(1R)-1-(4-chlorobenzyl)-2-methoxy-2-oxoethyl]amino}methyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

: 760167-36-0
N-{[(3R)-2-(tert-butoxycarbonyl)-1,2,3,4-tetrahydroisoquinolin-3-yl]methyl}-4-chloro-D-phenylalanine

Guidance literature:: tert-butyl (3R)-3-({[(1R)-1-(4-chlorobenzyl)-2-methoxy-2-oxoethyl]amino}methyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate; With methanol; lithium hydroxide; water; In tetrahydrofuran; at 0 ℃; for 19h;

With potassium hydrogensulfate; water; In tetrahydrofuran; methanol; pH=7;

Reference yield:

: endo-N-8-azabicyclo[3.2.1]oct-3-yl-N-cyclohexyl-N',N'-diethylurea

: 760167-36-0
N-{[(3R)-2-(tert-butoxycarbonyl)-1,2,3,4-tetrahydroisoquinolin-3-yl]methyl}-4-chloro-D-phenylalanine

: endo-tert-butyl (3R)-3-({[(1R)-1-(4-chlorobenzyl)-2-(3-{cyclohexyl[(diethylamino)carbonyl]amino}-8-azabicyclo[3.2.1]oct-8-yl)-2-oxoethyl]amino}methyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 16h;