2-Chloro-5-methoxyquinoxaline

Base Information

Chemical Name:2-Chloro-5-methoxyquinoxaline
CAS No.:76052-76-1
Molecular Formula:C9H7ClN2O
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID40506874
Wikidata:Q82362838

Synonyms:2-chloro-5-methoxyquinoxaline;76052-76-1;Quinoxaline, 2-chloro-5-methoxy-;SCHEMBL1039998;DTXSID40506874;BDA05276;MFCD26401268;AKOS027324155;AC-30570;BS-17493;CS-0161364;FT-0737762;C76433;A915108

Suppliers and Price of 2-Chloro-5-methoxyquinoxaline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-Chloro-5-methoxyquinoxaline

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:194.0246905
Heavy Atom Count:13
Complexity:179

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC2=NC(=CN=C21)Cl

Technology Process of 2-Chloro-5-methoxyquinoxaline

There total 4 articles about 2-Chloro-5-methoxyquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 924-44-7
glyoxylic acid ethyl ester

: 37466-89-0
3-methoxybenzene-1,2-diamine

: 659729-70-1
2-chloro-8-methoxyquinoxaline

: 76052-76-1
2-chloro-5-methoxy-quinoxaline

Guidance literature:: glyoxylic acid ethyl ester; 3-methoxybenzene-1,2-diamine; With sodium hydrogencarbonate;

With trichlorophosphate; Further stages.;
DOI:10.1016/j.bmcl.2007.10.055

Reference yield:

: 76052-79-4
5-methoxy-1H-quinoxalin-2-one

: 76052-76-1
2-chloro-5-methoxy-quinoxaline

Guidance literature:: With trichlorophosphate; In N,N-dimethyl-formamide; for 1.5h; Heating;
DOI:10.1021/jm00133a019

Reference yield:

: 37466-89-0
3-methoxybenzene-1,2-diamine

: 76052-76-1
2-chloro-5-methoxy-quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: 3 h / Ambient temperature

2: POCl₃ / dimethylformamide / 1.5 h / Heating

With trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00133a019