4,5-Dichloro-2-(methylamino)aniline

Base Information

Chemical Name:4,5-Dichloro-2-(methylamino)aniline
CAS No.:42450-33-9
Molecular Formula:C7H8Cl2N2
Molecular Weight:191.06
Hs Code.:2921590090
European Community (EC) Number:255-830-8
DSSTox Substance ID:DTXSID90195232
Nikkaji Number:J309.926A
Wikidata:Q83068113
Mol file:42450-33-9.mol

Synonyms:42450-33-9;4,5-Dichloro-2-(methylamino)aniline;4,5-Dichloro-N1-methylbenzene-1,2-diamine;EINECS 255-830-8;4,5-dichloro-2-N-methylbenzene-1,2-diamine;C7H8Cl2N2;SCHEMBL932424;C7-H8-Cl2-N2;DTXSID90195232;ZDMRZCPRJMRDQM-UHFFFAOYSA-N;2-(Methylamino)-4,5-dichloroaniline;AKOS017531811;N-methyl-4,5-dichloro-o-phenylenediamine;4,5-Dichloro-N-methylbenzene-1,2-diamine;FT-0759573;EN300-1721261;Z1262563876

Suppliers and Price of 4,5-Dichloro-2-(methylamino)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4,5-Dichloro-N1-methylbenzene-1,2-diamine 95+%
1g
$ 339.00

Alichem
4,5-Dichloro-N1-methylbenzene-1,2-diamine
1g
$ 400.00

Total 7 raw suppliers

Chemical Property of 4,5-Dichloro-2-(methylamino)aniline

Chemical Property:

Vapor Pressure:3.01E-05mmHg at 25°C
Boiling Point:356°Cat760mmHg
Flash Point:169.1°C
PSA：38.05000
Density:1.414g/cm³
LogP:3.27150
XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:190.0064537
Heavy Atom Count:11
Complexity:132

Purity/Quality:

99% ^*data from raw suppliers

4,5-Dichloro-N1-methylbenzene-1,2-diamine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CNC1=CC(=C(C=C1N)Cl)Cl

Technology Process of 4,5-Dichloro-2-(methylamino)aniline

There total 3 articles about 4,5-Dichloro-2-(methylamino)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 107342-18-7
4,5-dichloro-N-methyl-2-nitrobenzenamine

: 42450-33-9
4,5-dichloro-N¹-methylbenzene-1,2-diamine

Guidance literature:: With iron; acetic acid; In ethanol; at 60 ℃; for 2h;
DOI:10.3390/molecules25122855

Reference yield:

: 2339-78-8
1,2-dichloro-4-fluoro-5-nitrobenzene

: 42450-33-9
4,5-dichloro-N¹-methylbenzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / CH₂Cl₂; H₂O / 14 h / 20 °C

2: H₂ / Raney Ni / 5 h / 20 °C

With hydrogen; potassium carbonate; nickel; In dichloromethane; water;
DOI:10.1016/S0040-4039(02)01754-9

Reference yield:

: 6641-64-1
4,5-dichloro-2-nitroaniline

: 42450-33-9
4,5-dichloro-N¹-methylbenzene-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; tetrabutylammomium bromide / toluene / 5 h / 20 °C

2: iron; ammonium chloride / water; ethanol / 48 h / 60 - 80 °C

With tetrabutylammomium bromide; iron; ammonium chloride; sodium hydroxide; In ethanol; water; toluene;