1,1'-Oxybis(4-ethenylbenzene)

Base Information

• Chemical Name: 1,1'-Oxybis(4-ethenylbenzene)
• CAS No.: 7659-54-3
• Molecular Formula: C16H14O
• Molecular Weight: 222.287
• DSSTox Substance ID: DTXSID20488780
• Nikkaji Number: J730.962G
• Wikidata: Q82331659

Synonyms:1,1'-oxybis(4-ethenylbenzene);7659-54-3;Benzene, 1,1'-oxybis[4-ethenyl-;1-ETHENYL-4-(4-ETHENYLPHENOXY)BENZENE;bis(4-vinylphenyl) ether;SCHEMBL296908;DTXSID20488780

Chemical Property of 1,1'-Oxybis(4-ethenylbenzene)

Chemical Property:

• XLogP3: 5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 222.104465066
• Heavy Atom Count: 17
• Complexity: 216

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CC1=CC=C(C=C1)OC2=CC=C(C=C2)C=C

Technology Process of 1,1'-Oxybis(4-ethenylbenzene)

There total 9 articles about 1,1'-Oxybis(4-ethenylbenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-Vinylphenylboronic acid (2156-04-9,593231-72-2) + phenylacetylene (536-74-3) → 1,4-diphenyl-1,3-butadiyne (886-66-8) + 4,4'-divinyldiphenyl ether (7659-54-3) + 1-(phenylethynyl)-4-vinylbenzene (3365-10-4)

Guidance literature:

4-Vinylphenylboronic acid; With copper diacetate; triethylamine; In dichloromethane; water; at 20 ℃; for 1h;

phenylacetylene; In dichloromethane; water; at 20 ℃; for 48h;

DOI:10.1021/acschembio.6b00685

Reference yield:

2-methyl-acrylic acid 1-(4-{4-[1-(2-methyl-acryloyloxy)-ethyl]-phenoxy}-phenyl)-ethyl ester (82576-72-5) → poly(bis[4-(1-hydroxyethyl)phenyl] ether dimethacrylate) + poly(methacrylic acid) (79-41-4,25087-26-7,50867-57-7) + 4,4'-divinyldiphenyl ether (7659-54-3) + 4-vinylphenyl-4-(1-methacryloyloxyethyl)phenyl ether (70817-54-8)

Guidance literature:

at 140 ℃; Further Variations:; Temperatures; Product distribution;

DOI:10.1023/B:RJAC.0000015734.96608.da

Reference yield:

bis<4-(1-hydroxyethyl)phenyl> ether (5325-82-6) → 4,4'-divinyldiphenyl ether (7659-54-3)

Guidance literature:

With toluene-4-sulfonic acid; In o-xylene; water; Reflux;

DOI:10.1134/S1070427210070190

upstream raw materials:

bis<4-(1-isopropoxyethyl)phenyl> ether

bis<4-(1-ethoxyethyl)phenyl> ether

poly(methacrylic acid)

bis<4-(1-hydroxyethyl)phenyl> ether

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