Pyrido[2,3-d]pyrimidine-2,4(3H,8H)-dione, 8-(2-hydroxyethyl)-7-methyl-6-(phenylmethyl)-

Base Information

Chemical Name:Pyrido[2,3-d]pyrimidine-2,4(3H,8H)-dione, 8-(2-hydroxyethyl)-7-methyl-6-(phenylmethyl)-
CAS No.:76641-34-4
Molecular Formula:C₁₇H₁₇N₃O₃
Molecular Weight:311.34
Hs Code.:

Synonyms:

Suppliers and Price of Pyrido[2,3-d]pyrimidine-2,4(3H,8H)-dione, 8-(2-hydroxyethyl)-7-methyl-6-(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Pyrido[2,3-d]pyrimidine-2,4(3H,8H)-dione, 8-(2-hydroxyethyl)-7-methyl-6-(phenylmethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Pyrido[2,3-d]pyrimidine-2,4(3H,8H)-dione, 8-(2-hydroxyethyl)-7-methyl-6-(phenylmethyl)-

There total 5 articles about Pyrido[2,3-d]pyrimidine-2,4(3H,8H)-dione, 8-(2-hydroxyethyl)-7-methyl-6-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 76641-73-1
2-benzyl-3,3-ethylenedioxybutanal

: 5770-52-5
6-(2-hydroxyethylamino)pyrimidine-2,4(1H,3H)-dione

: 76641-34-4
6-benzyl-8-(2-hydroxyethyl)-7-methylpyrido<2,3-d>pyrimidine-2,4(3H,8H)-dione

Guidance literature:: With hydrogenchloride; In ethanol; water; at 100 ℃; for 4h;

Reference yield:

: 620-80-4
ethyl 2-benzylidene acetoacetate

: 76641-34-4
6-benzyl-8-(2-hydroxyethyl)-7-methylpyrido<2,3-d>pyrimidine-2,4(3H,8H)-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / H₂ / palladium on charcoal / ethyl acetate / 0.5 h / 2280 Torr

2: 90 percent / toluene-p-sulphonic acid / benzene / 22 h / Heating

3: 90 percent / LiAlH₄ / diethyl ether / 60 h / Ambient temperature

4: 82 percent / chromium trioxide, pyridine / CH₂Cl₂ / 2.5 h / 20 °C

5: 30 percent / HCl / H₂O; ethanol / 4 h / 100 °C

With pyridine; chromium(VI) oxide; hydrogenchloride; lithium aluminium tetrahydride; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; water; ethyl acetate; benzene;

Reference yield:

: 76641-71-9
2-(2-Methyl-1,3-dioxolanyl)-3-phenyl-propansaeureethylester

: 76641-34-4
6-benzyl-8-(2-hydroxyethyl)-7-methylpyrido<2,3-d>pyrimidine-2,4(3H,8H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / LiAlH₄ / diethyl ether / 60 h / Ambient temperature

2: 82 percent / chromium trioxide, pyridine / CH₂Cl₂ / 2.5 h / 20 °C

3: 30 percent / HCl / H₂O; ethanol / 4 h / 100 °C

With pyridine; chromium(VI) oxide; hydrogenchloride; lithium aluminium tetrahydride; In diethyl ether; ethanol; dichloromethane; water;