2-aMinophenyl Methanesulfonate

Base Information

Chemical Name:2-aMinophenyl Methanesulfonate
CAS No.:77153-74-3
Molecular Formula:C7H9NO3S
Molecular Weight:187.22
Hs Code.:
Mol file:77153-74-3.mol

Synonyms:2-aMinophenyl Methanesulfonate;Phenol, 2-amino-, 1-methanesulfonate

Suppliers and Price of 2-aMinophenyl Methanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-AMINOPHENYL METHANESULFONATE 95.00%
5MG
$ 502.23

Total 4 raw suppliers

Chemical Property of 2-aMinophenyl Methanesulfonate

Chemical Property:

PSA：79.44000
LogP:7.68020

Purity/Quality:

99% ^*data from raw suppliers

2-AMINOPHENYL METHANESULFONATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-aMinophenyl Methanesulfonate

There total 2 articles about 2-aMinophenyl Methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 144167-32-8
N-(2-mesyloxyphenyl)-α-carbethoxyamidine

: 77153-74-3
2-aminophenyl methanesulfonate

: 144167-37-3
o-mesyloxyformanilide

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In ethanol; water; for 40h; Heating;
DOI:10.1016/S0040-4020(01)88224-7

Reference yield:

: 144167-25-9
α-amino-α-carbethoxy-N-phenylnitrone

: 77153-74-3
2-aminophenyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

2: 62 percent / DABCO / ethanol; H₂O / 40 h / Heating; or in EtOD, D₂O

With 1,4-diaza-bicyclo[2.2.2]octane; triethylamine; In ethanol; dichloromethane; water;
DOI:10.1016/S0040-4020(01)88224-7