1,2-Diazacycloheptane

Base Information

Chemical Name:1,2-Diazacycloheptane
CAS No.:5700-00-5
Molecular Formula:C₅H₁₂N₂
Molecular Weight:100.164
Hs Code.:
DSSTox Substance ID:DTXSID901335966
Nikkaji Number:J1.119.997F

Synonyms:1,2-diazacycloheptane;1,2-diazepane;[1,2]diazepane;5700-00-5;SCHEMBL123864;DTXSID901335966

Suppliers and Price of 1,2-Diazacycloheptane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 1,2-Diazacycloheptane

Chemical Property:

XLogP3:0.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:100.100048391
Heavy Atom Count:7
Complexity:39.3

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCNNCC1

Technology Process of 1,2-Diazacycloheptane

There total 1 articles about 1,2-Diazacycloheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-46-9
benzylamine

: 218947-49-0
2-[(3-chloro-propyl)-(4-methoxy-benzenesulfonyl)-amino]-acrylic acid methyl ester

: 5700-00-5
perhydrodiazepine

: 218947-50-3
4-benzyl-1-(4-methoxy-benzenesulfonyl)-[1,4]diazepane-2-carboxylic acid methyl ester

Guidance literature:: With sodium iodide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

Reference yield:

: 5700-00-5
perhydrodiazepine

: 137250-77-2
(3S,4R)-3,4-Diphenyl-1,6-diaza-cycloundecane-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / tetrahydrofuran; H₂O

2: i-Pr₂NH; n-BuLi / tetrahydrofuran; hexane / 6 h / -78 - 50 °C

With n-butyllithium; potassium carbonate; diisopropylamine; In tetrahydrofuran; hexane; water; 1: Acylation / 2: anionic <3,3> rearrangement;
DOI:10.3987/COM-99-8747

Reference yield:

: 5700-00-5
perhydrodiazepine

: 137250-76-1,137250-77-2
(3S,4S)-3,4-Diphenyl-1,6-diaza-cycloundecane-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / tetrahydrofuran; H₂O

2: i-Pr₂NH; n-BuLi / tetrahydrofuran; hexane / 6 h / -78 - 50 °C

With n-butyllithium; potassium carbonate; diisopropylamine; In tetrahydrofuran; hexane; water; 1: Acylation / 2: anionic <3,3> rearrangement;
DOI:10.3987/COM-99-8747