1,3-Propanediol, 2-(cyclohexylidenemethyl)-

Base Information

Chemical Name:1,3-Propanediol, 2-(cyclohexylidenemethyl)-
CAS No.:77192-46-2
Molecular Formula:C10H18O2
Molecular Weight:170.252
Hs Code.:
DSSTox Substance ID:DTXSID00452505

Synonyms:77192-46-2;1,3-Propanediol, 2-(cyclohexylidenemethyl)-;DTXSID00452505

Suppliers and Price of 1,3-Propanediol, 2-(cyclohexylidenemethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Propanediol, 2-(cyclohexylidenemethyl)-

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:170.130679813
Heavy Atom Count:12
Complexity:140

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC(=CC(CO)CO)CC1

Technology Process of 1,3-Propanediol, 2-(cyclohexylidenemethyl)-

There total 7 articles about 1,3-Propanediol, 2-(cyclohexylidenemethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 71310-20-8
ethyl 2-ethyloxycarbonyl-3-cyclohexyliden-propanoate

: 77192-46-2
2-hydroxymethyl-3-cyclohexyliden-propan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo8020659

Reference yield: 43.2%

: 77192-35-9
3-Cyclohexylidenemethyl-oxetan-2-one

: 77192-46-2
2-hydroxymethyl-3-cyclohexyliden-propan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1039/P19810000270

Reference yield:

: 13592-76-2
diethyl 2-(cyclohexylmethylene)malonate

: 77192-46-2
2-hydroxymethyl-3-cyclohexyliden-propan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / NaH / tetrahydrofuran / a.) 0 deg C, b.) 50 deg C, 20 h

2: LiAlH₄ / diethyl ether / a.) 0 deg C, b.) room temperature

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00031a039