Diethyl (cyclohexylidenemethyl)propanedioate

Base Information

Chemical Name:Diethyl (cyclohexylidenemethyl)propanedioate
CAS No.:71310-20-8
Molecular Formula:C14H22O4
Molecular Weight:254.326
Hs Code.:
DSSTox Substance ID:DTXSID70499664

Synonyms:Diethyl (cyclohexylidenemethyl)propanedioate;71310-20-8;DTXSID70499664

Suppliers and Price of Diethyl (cyclohexylidenemethyl)propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diethyl (cyclohexylidenemethyl)propanedioate

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:254.15180918
Heavy Atom Count:18
Complexity:294

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)C(C=C1CCCCC1)C(=O)OCC

Technology Process of Diethyl (cyclohexylidenemethyl)propanedioate

There total 4 articles about Diethyl (cyclohexylidenemethyl)propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 13592-76-2
diethyl 2-(cyclohexylmethylene)malonate

: 71310-20-8
ethyl 2-ethyloxycarbonyl-3-cyclohexyliden-propanoate

Guidance literature:: With 2-(N,N-dimethylamino)ethanol; In dichloromethane; at 0 ℃; Inert atmosphere; UV-irradiation;
DOI:10.1021/jo8020659

Reference yield:

: 105-53-3
diethyl malonate

: 71310-20-8
ethyl 2-ethyloxycarbonyl-3-cyclohexyliden-propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / piperidinium acetate / benzene / Heating

2: 50 percent / NaH / tetrahydrofuran / a.) 0 deg C, b.) 50 deg C, 20 h

With piperdinium acetate; sodium hydride; In tetrahydrofuran; benzene;
DOI:10.1021/jo00031a039

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 71310-20-8
ethyl 2-ethyloxycarbonyl-3-cyclohexyliden-propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / piperidinium acetate / benzene / Heating

2: 50 percent / NaH / tetrahydrofuran / a.) 0 deg C, b.) 50 deg C, 20 h

With piperdinium acetate; sodium hydride; In tetrahydrofuran; benzene;
DOI:10.1021/jo00031a039