4-((4-Chlorophenyl)sulfonyl)benzaldehyde

Base Information

Chemical Name:4-((4-Chlorophenyl)sulfonyl)benzaldehyde
CAS No.:77422-24-3
Molecular Formula:C13H9ClO3S
Molecular Weight:280.732
Hs Code.:2913000090
European Community (EC) Number:673-318-6
DSSTox Substance ID:DTXSID20355201
Nikkaji Number:J3.452.796B
Wikidata:Q72457565
Mol file:77422-24-3.mol

Synonyms:77422-24-3;4-((4-Chlorophenyl)sulfonyl)benzaldehyde;4-(4-Chlorobenzenesulfonyl)benzaldehyde;4-(4-Chlorophenylsulfonyl)benzaldehyde;4-(4-chlorophenyl)sulfonylbenzaldehyde;4-[(4-chlorophenyl)sulfonyl]benzaldehyde;Cambridge id 5307564;Oprea1_235898;Oprea1_266114;SCHEMBL1024421;DTXSID20355201;FVBVLYDUSHDJOK-UHFFFAOYSA-N;CDA42224;CK2508;MFCD00444606;AKOS000541299;AS-45918;4-(4-Chlorobenzene-1-sulfonyl)benzaldehyde;CS-0326405;AB00079818-01;A1-08683

Suppliers and Price of 4-((4-Chlorophenyl)sulfonyl)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4-((4-Chlorophenyl)sulfonyl)benzaldehyde 95+%
1g
$ 455.00

American Custom Chemicals Corporation
4-(4-CHLOROBENZENESULFONYL)BENZALDEHYDE 95.00%
5MG
$ 505.68

Alichem
4-((4-Chlorophenyl)sulfonyl)benzaldehyde
1g
$ 405.48

AK Scientific
4-(4-Chlorobenzenesulfonyl)benzaldehyde
250mg
$ 496.00

AK Scientific
4-(4-Chlorobenzenesulfonyl)benzaldehyde
1g
$ 1171.00

AHH
4-(4-Chlorobenzenesulfonyl)benzaldehyde 98%
5g
$ 830.00

A1 Biochem Labs
4-(4-Chlorobenzenesulfonyl)benzaldehyde 95%
2.5 g
$ 950.00

Total 12 raw suppliers

Chemical Property of 4-((4-Chlorophenyl)sulfonyl)benzaldehyde

Chemical Property:

Melting Point:154℃
PSA：59.59000
Density:1.393
LogP:4.06610
XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:279.9960930
Heavy Atom Count:18
Complexity:372

Purity/Quality:

98%min ^*data from raw suppliers

4-((4-Chlorophenyl)sulfonyl)benzaldehyde 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C=O)S(=O)(=O)C2=CC=C(C=C2)Cl

Technology Process of 4-((4-Chlorophenyl)sulfonyl)benzaldehyde

There total 4 articles about 4-((4-Chlorophenyl)sulfonyl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 137736-07-3
4-(4-chloro-phenylsulfanyl)-benzaldehyde

: 77422-24-3
4-(4-chlorobenzenesulfonyl)benzaldehyde

Guidance literature:: With aluminum oxide; sodium periodate; Ru/Al₂O₃; In water; for 2h; Green chemistry;
DOI:10.1055/s-0035-1560834

Reference yield: 82.0%

: 14752-66-0
sodium p-chlorobenzenesulphinate

: 555-16-8
4-nitrobenzaldehdye

: 77422-24-3
4-(4-chlorobenzenesulfonyl)benzaldehyde

Guidance literature:: With {(Pd{Fe(η5-C5H5)(η5-C5H3C(CH3)=NC6H4CH3-4)}(μ-Cl))2}; potassium carbonate; In dimethyl sulfoxide; at 110 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2014.09.087

Reference yield:

: 98-60-2
4-chlorobenzenesulfonyl chloride

: 77422-24-3
4-(4-chlorobenzenesulfonyl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfite; sodium hydrogencarbonate / water / 4 h / 70 - 80 °C

2: {(Pd{Fe(η5-C5H5)(η5-C5H3C(CH3)=NC6H4CH3-4)}(μ-Cl))2}; potassium carbonate / dimethyl sulfoxide / 12 h / 110 °C / Inert atmosphere

With {(Pd{Fe(η5-C5H5)(η5-C5H3C(CH3)=NC6H4CH3-4)}(μ-Cl))2}; sodium hydrogencarbonate; potassium carbonate; sodium sulfite; In water; dimethyl sulfoxide;
DOI:10.1016/j.tet.2014.09.087