Pyrimido[5,4-d]pyrimidine-4,8-diamine, N,N,N',N'-tetrakis[(3,4-dimethoxyphenyl)methyl]-2,6-bis[3-[[tris(1-methyl ethyl)silyl]oxy]propoxy]-

Base Information

Chemical Name:Pyrimido[5,4-d]pyrimidine-4,8-diamine, N,N,N',N'-tetrakis[(3,4-dimethoxyphenyl)methyl]-2,6-bis[3-[[tris(1-methyl ethyl)silyl]oxy]propoxy]-
CAS No.:774539-27-4
Molecular Formula:C66H98N6O12Si2
Molecular Weight:1223.71
Hs Code.:

Pyrimido[5,4-d]pyrimidine-4,8-diamine,
N,N,N',N'-tetrakis[(3,4-dimethoxyphenyl)methyl]-2,6-bis[3-[[tris(1-methyl
ethyl)silyl]oxy]propoxy]-

Synonyms:

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Chemical Property of Pyrimido[5,4-d]pyrimidine-4,8-diamine, N,N,N',N'-tetrakis[(3,4-dimethoxyphenyl)methyl]-2,6-bis[3-[[tris(1-methyl ethyl)silyl]oxy]propoxy]-

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Technology Process of Pyrimido[5,4-d]pyrimidine-4,8-diamine, N,N,N',N'-tetrakis[(3,4-dimethoxyphenyl)methyl]-2,6-bis[3-[[tris(1-methyl ethyl)silyl]oxy]propoxy]-

There total 7 articles about Pyrimido[5,4-d]pyrimidine-4,8-diamine, N,N,N',N'-tetrakis[(3,4-dimethoxyphenyl)methyl]-2,6-bis[3-[[tris(1-methyl ethyl)silyl]oxy]propoxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 178905-39-0
3-[1,1-bis(methylethyl)-2-methyl-1-silapropoxy]propane-1-ol

: 270920-52-0
2,6-dichloro-4,8-bis-[di-N,N-(3',4'-dimethoxybenzyl)amino]pyrimido[5,4-d]pyrimidine

: 774539-27-4
2,6-di-(3'-triisopropylsilyloxypropoxy)-4,8-bis(di-N,N-(3',4'-dimethoxybenzyl)amino)pyrimido[5,4-d]pyrimidine

Guidance literature:: 3-[1,1-bis(methylethyl)-2-methyl-1-silapropoxy]propane-1-ol; With sodium hydride; In tetrahydrofuran; at 60 ℃; for 0.0833333h;

2,6-dichloro-4,8-bis-[di-N,N-(3',4'-dimethoxybenzyl)amino]pyrimido[5,4-d]pyrimidine; In tetrahydrofuran; Heating;
DOI:10.1021/jm040772w

Reference yield:

: 32980-71-5
2,4,6,8-Tetrachloro-pyrimido[5,4-d]pyrimidine

: 774539-27-4
2,6-di-(3'-triisopropylsilyloxypropoxy)-4,8-bis(di-N,N-(3',4'-dimethoxybenzyl)amino)pyrimido[5,4-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 68 percent / K₂CO₃ / tetrahydrofuran / 25 °C

2.1: NaH / tetrahydrofuran / 0.08 h / 60 °C

2.2: 65 percent / tetrahydrofuran / Heating

With sodium hydride; potassium carbonate; In tetrahydrofuran;
DOI:10.1021/jm040772w

Reference yield:

: 5634-21-9
N,N-bis-(3,4-dimethoxybenzyl)amine

: 774539-27-4
2,6-di-(3'-triisopropylsilyloxypropoxy)-4,8-bis(di-N,N-(3',4'-dimethoxybenzyl)amino)pyrimido[5,4-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 68 percent / K₂CO₃ / tetrahydrofuran / 25 °C

2.1: NaH / tetrahydrofuran / 0.08 h / 60 °C

2.2: 65 percent / tetrahydrofuran / Heating

With sodium hydride; potassium carbonate; In tetrahydrofuran;
DOI:10.1021/jm040772w