2-(Bromomethyl)-1,2,3,4-tetrahydronaphthalene

Base Information

Chemical Name:2-(Bromomethyl)-1,2,3,4-tetrahydronaphthalene
CAS No.:77508-59-9
Molecular Formula:C11H13Br
Molecular Weight:225.12500
Hs Code.:
DSSTox Substance ID:DTXSID80508115

Synonyms:2-(Bromomethyl)-1,2,3,4-tetrahydronaphthalene;77508-59-9;Naphthalene, 2-(bromomethyl)-1,2,3,4-tetrahydro-;SCHEMBL1689635;DTXSID80508115;MUGPULGJDGEABF-UHFFFAOYSA-N;AKOS015152614;2-Bromomethyl-1,2,3,4-tetrahydronaphthalene;EN300-130243

Suppliers and Price of 2-(Bromomethyl)-1,2,3,4-tetrahydronaphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
2-(Bromomethyl)-1,2,3,4-tetrahydronaphthalene
2.5g
$ 1570.00

Total 3 raw suppliers

Chemical Property of 2-(Bromomethyl)-1,2,3,4-tetrahydronaphthalene

Chemical Property:

PSA：0.00000
LogP:3.18640
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:224.02006
Heavy Atom Count:12
Complexity:144

Purity/Quality:

99% ^*data from raw suppliers

2-(Bromomethyl)-1,2,3,4-tetrahydronaphthalene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=CC=CC=C2CC1CBr

Technology Process of 2-(Bromomethyl)-1,2,3,4-tetrahydronaphthalene

There total 5 articles about 2-(Bromomethyl)-1,2,3,4-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.6%

: 6947-15-5
1,2,3,4-tetrahydro-2-naphthalene methanol

: 77508-59-9
2-bromomethyl-1,2,3,4-tetrahydro-2-naphthalene

Guidance literature:: With phosphorus tribromide; In dichloromethane;

Reference yield:

: Trifluoro-acetic acid 1,2,3,4-tetrahydro-naphthalen-2-ylmethyl ester

: 77508-59-9
2-bromomethyl-1,2,3,4-tetrahydro-2-naphthalene

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium bromide; In tetrahydrofuran; for 6h; Yield given; Heating;

Reference yield:

: 39246-30-5
methyl 1,2,3,4-tetrahydronaphthalene-2-carboxylate

: 77508-59-9
2-bromomethyl-1,2,3,4-tetrahydro-2-naphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

2: 0.25 h / Ambient temperature

3: LiBr, hexamethylphosphoric triamide (HMPA) / tetrahydrofuran / 6 h / Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; lithium bromide; In tetrahydrofuran; diethyl ether;