Benzene, 1-(ethenyloxy)-2-methoxy-

Base Information

• Chemical Name: Benzene, 1-(ethenyloxy)-2-methoxy-
• CAS No.: 7784-99-8
• Molecular Formula: C9H10O2
• Molecular Weight: 150.177
• DSSTox Substance ID: DTXSID50466051
• Nikkaji Number: J799.336F
• Wikidata: Q82292430
• Mol file: 7784-99-8.mol

Synonyms:Benzene, 1-(ethenyloxy)-2-methoxy-;7784-99-8;methox yphenol vinyl ether;SCHEMBL779616;JCIXLSHBTLKMCB-UHFFFAOYSA-;DTXSID50466051;AKOS015714096;InChI=1/C9H10O2/c1-3-11-9-7-5-4-6-8(9)10-2/h3-7H,1H2,2H3

Chemical Property of Benzene, 1-(ethenyloxy)-2-methoxy-

Chemical Property:

• Vapor Pressure: 0.0841mmHg at 25°C
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 150.068079557
• Heavy Atom Count: 11
• Complexity: 123

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=CC=C1OC=C

Technology Process of Benzene, 1-(ethenyloxy)-2-methoxy-

There total 9 articles about Benzene, 1-(ethenyloxy)-2-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C14H21NO3 → 1-methoxy-2-vinyloxybenzene (7784-99-8)

Guidance literature:

With N,O-bis-(trimethylsilyl)-acetamide; In toluene; for 0.5h; Reflux;

DOI:10.1016/j.tet.2021.132108

Reference yield: 70.0%

2-methoxy-phenol (90-05-1) + 2,4,6-trivinylcyclotriboroxane*pyridine complex → 1-methoxy-2-vinyloxybenzene (7784-99-8)

Guidance literature:

With pyridine; copper diacetate; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1021/jo049314l

Reference yield:

C15H15O4PolS → 1-methoxy-2-vinyloxybenzene (7784-99-8)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 0.133333h; solid phase reaction;

DOI:10.1002/cjoc.201100451

upstream raw materials:

1-(2-chloroethoxy)-2-methoxybenzene

2-methoxy-phenol

1,2-dichloro-ethane

acetylene

Downstream raw materials:

2-(2-Methoxy-phenoxy)-propionaldehyde

dibutyl acetal

2-methoxy-phenol