[4-(Dimethylamino)phenyl]phosphonic dichloride

Base Information

Chemical Name:[4-(Dimethylamino)phenyl]phosphonic dichloride
CAS No.:77918-53-7
Molecular Formula:C8H10Cl2NOP
Molecular Weight:238.05100
Hs Code.:
DSSTox Substance ID:DTXSID30506343
Wikidata:Q82362048

Synonyms:77918-53-7;[4-(Dimethylamino)phenyl]phosphonic dichloride;SCHEMBL11217437;DTXSID30506343

Suppliers and Price of [4-(Dimethylamino)phenyl]phosphonic dichloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of [4-(Dimethylamino)phenyl]phosphonic dichloride

Chemical Property:

Melting Point:120-121 °C
Boiling Point:326.4±25.0 °C(Predicted)
PSA：30.12000
Density:1.33±0.1 g/cm3(Predicted)
LogP:3.04860
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:236.9877063
Heavy Atom Count:13
Complexity:208

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1=CC=C(C=C1)P(=O)(Cl)Cl

Technology Process of [4-(Dimethylamino)phenyl]phosphonic dichloride

There total 2 articles about [4-(Dimethylamino)phenyl]phosphonic dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 29972-74-5
(4-dimethylamino-phenyl)-phosphonous acid dichloride

: 77918-53-7
p-dimethylaminophenylphosphonic acid dichloride

Guidance literature:: With dimethyl sulfoxide; In dichloromethane; at -70 ℃; for 1.5h;

Reference yield:

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 77918-53-7
p-dimethylaminophenylphosphonic acid dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / phosphorustrichloride

2: dimethylsulfoxide

With dimethyl sulfoxide; phosphorus trichloride;