Benzaldehyde, 4-bromo-2,5-dipropyl-

Base Information

Chemical Name:Benzaldehyde, 4-bromo-2,5-dipropyl-
CAS No.:782236-42-4
Molecular Formula:C13H17BrO
Molecular Weight:269.17700
Hs Code.:
DSSTox Substance ID:DTXSID10478337
Wikidata:Q82311664

Synonyms:Benzaldehyde, 4-bromo-2,5-dipropyl-;782236-42-4;DTXSID10478337

Suppliers and Price of Benzaldehyde, 4-bromo-2,5-dipropyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzaldehyde, 4-bromo-2,5-dipropyl-

Chemical Property:

PSA：17.07000
LogP:4.16660
XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:268.04628
Heavy Atom Count:15
Complexity:193

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC1=CC(=C(C=C1Br)CCC)C=O

Technology Process of Benzaldehyde, 4-bromo-2,5-dipropyl-

There total 1 articles about Benzaldehyde, 4-bromo-2,5-dipropyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 40820-32-4
1,4-dibromo-2,5-dipropylbenzene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 782236-42-4
4-bromo-2,5-dipropylbenzaldehyde

Guidance literature:: 1,4-dibromo-2,5-dipropylbenzene; With n-butyllithium; In tetrahydrofuran; at -70 - -60 ℃;

N,N-dimethyl-formamide; In tetrahydrofuran; at -60 - 20 ℃;
DOI:10.1021/jo049111x

Reference yield: 96.0%

: 782236-42-4
4-bromo-2,5-dipropylbenzaldehyde

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 862974-50-3
2-(4-bromo-2,5-dipropylphenyl)-5,5-dimethyl[1,3]dioxane

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 2h; Heating;
DOI:10.1021/jo0506783

Reference yield:

: 782236-42-4
4-bromo-2,5-dipropylbenzaldehyde

: (4-{2-[4-(5,5-dimethyl-1,3-dioxan-2-yl)-2,5-dipropylphenyl]vinyl}benzyl)phosphonic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; tri-tert-butylphosphine tetrafluoroboric acid salt / Pd₂(dba)3 / dioxane

2: p-toluenesulfonic acid / toluene

With toluene-4-sulfonic acid; triethylamine; tri tert-butylphosphoniumtetrafluoroborate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In 1,4-dioxane; toluene; 1: Heck reaction;
DOI:10.1021/jo0506783