N-[3-(diethylamino)propyl]acetamide

Base Information

• Chemical Name: N-[3-(diethylamino)propyl]acetamide
• CAS No.: 32039-09-1
• Molecular Formula: C9H20 N2 O
• Molecular Weight: 172.2679
• Mol file: 32039-09-1.mol

Synonyms:NSC 165777

Chemical Property of N-[3-(diethylamino)propyl]acetamide

Chemical Property:

• Vapor Pressure: 0.0011mmHg at 25°C
• Boiling Point: 300.8°Cat760mmHg
• Flash Point: 135.7°C
• Density: 0.905g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-[3-(diethylamino)propyl]acetamide

There total 2 articles about N-[3-(diethylamino)propyl]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

acetic anhydride (108-24-7) + diethylaminopropylamine (104-78-9) → 3-diethylaminopropyl-1-acetamide (32039-09-1)

Guidance literature:

With pyridine; for 18h; Ambient temperature;

DOI:10.1248/cpb.45.996

Reference yield:

→ 3-diethylaminopropyl-1-acetamide (32039-09-1)

Guidance literature:

/BRN= 741879/, Acetanhydrid, Pyridin;

DOI:10.1002/oms.1210130105

Reference yield: 92.0%

3-diethylaminopropyl-1-acetamide (32039-09-1) → N,N,N'-triethylpropylenediamine (22268-51-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 80 ℃; for 1h;

DOI:10.1248/cpb.45.996

upstream raw materials:

acetic anhydride

diethylaminopropylamine

Downstream raw materials:

N,N,N'-triethylpropylenediamine