Phosphonium, [3-(1-methoxy-1-methylethoxy)propyl]triphenyl-, bromide

Base Information

Chemical Name:Phosphonium, [3-(1-methoxy-1-methylethoxy)propyl]triphenyl-, bromide
CAS No.:78606-74-3
Molecular Formula:C25H30O2P.Br
Molecular Weight:473.39
Hs Code.:
DSSTox Substance ID:DTXSID50449445

Synonyms:78606-74-3;Phosphonium, [3-(1-methoxy-1-methylethoxy)propyl]triphenyl-, bromide;SCHEMBL9574126;DTXSID50449445;DKMRZUHVDROMTM-UHFFFAOYSA-M;[3-(1-methoxy-1-methylethoxy)propyl] triphenylphosphonium bromide;[3-(1-methoxy-1-methylethoxy)propyl](triphenylphosphonium)bromide

Suppliers and Price of Phosphonium, [3-(1-methoxy-1-methylethoxy)propyl]triphenyl-, bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Phosphonium, [3-(1-methoxy-1-methylethoxy)propyl]triphenyl-, bromide

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:9
Exact Mass:472.11668
Heavy Atom Count:29
Complexity:386

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(OC)OCCC[P+](C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3.[Br-]

Technology Process of Phosphonium, [3-(1-methoxy-1-methylethoxy)propyl]triphenyl-, bromide

There total 1 articles about Phosphonium, [3-(1-methoxy-1-methylethoxy)propyl]triphenyl-, bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 116-11-0
2-Methoxypropene

: 51860-45-8
3-hydroxypropyltriphenylphosphonium bromide

: 78606-74-3
2-methoxy-2-propyl ether of (3-hydroxy propyl)triphenylphosphonium bromide

Guidance literature:: pyridinium p-toluenesulfonate; In dichloromethane; at -30 ℃; for 3h;
DOI:10.1016/S0040-4039(01)90241-2

Reference yield:

: 4397-53-9
p-benzyloxybenzaldehyde

: 78606-74-3
2-methoxy-2-propyl ether of (3-hydroxy propyl)triphenylphosphonium bromide

: 4-[4-(Phenylmethoxy)phenyl]-3-butenol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; THF-water-2 M hydrochloric acid; hexane;

Reference yield:

: 78606-74-3
2-methoxy-2-propyl ether of (3-hydroxy propyl)triphenylphosphonium bromide

: 79065-01-3
[(3Z,7Z)-(R)-5-(tert-Butyl-dimethyl-silanyloxy)-trideca-3,7-dienyl]-triphenyl-phosphonium; iodide

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium, hexamethylphosphoric triamide / 1.) THF, -78 deg C, 30 min; -78 deg C -> 0 deg C, 60 min, 2.) pH 4 buffer, 25 deg C, 24 h

3: acetonitrile / 21 h / 60 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In acetonitrile;
DOI:10.1021/ja00547a600