Thiomorpholine, 4-[4-[(4-methoxyphenyl)azo]phenyl]-, 1,1-dioxide

Base Information

• Chemical Name: Thiomorpholine, 4-[4-[(4-methoxyphenyl)azo]phenyl]-, 1,1-dioxide
• CAS No.: 78866-05-4
• Molecular Formula: C₁₇H₁₉N₃O₃S
• Molecular Weight: 345.422
• Mol file: 78866-05-4.mol

Synonyms:

Chemical Property of Thiomorpholine, 4-[4-[(4-methoxyphenyl)azo]phenyl]-, 1,1-dioxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Thiomorpholine, 4-[4-[(4-methoxyphenyl)azo]phenyl]-, 1,1-dioxide

There total 2 articles about Thiomorpholine, 4-[4-[(4-methoxyphenyl)azo]phenyl]-, 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aniline (62-53-3) → [4-(1,1-Dioxo-1λ6-thiomorpholin-4-yl)-phenyl]-(4-methoxy-phenyl)-diazene (78866-05-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 30 percent

2: 1.) NaNO₂, 2.) acetic acid / 1.) H₂O, 0 deg C, 2.) 0 deg C, 3 h

With acetic acid; sodium nitrite;

DOI:10.1039/P29860000123

Reference yield:

4-Phenyltetrahydro-1,4-thiazine 1,1-dioxide (17688-68-5) + 4-methoxy-aniline (104-94-9) → [4-(1,1-Dioxo-1λ6-thiomorpholin-4-yl)-phenyl]-(4-methoxy-phenyl)-diazene (78866-05-4)

Guidance literature:

With acetic acid; sodium nitrite; Yield given. Multistep reaction; 1.) H₂O, 0 deg C, 2.) 0 deg C, 3 h;

DOI:10.1039/P29860000123

upstream raw materials:

4-Phenyltetrahydro-1,4-thiazine 1,1-dioxide

4-methoxy-aniline

aniline

Refernces