2,3-Dimethoxy-9-acridinone

Base Information

Chemical Name:2,3-Dimethoxy-9-acridinone
CAS No.:86640-16-6
Molecular Formula:C₁₅H₁₃NO₃
Molecular Weight:255.273
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-Dimethoxy-9-acridinone

Chemical Property:

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Technology Process of 2,3-Dimethoxy-9-acridinone

There total 1 articles about 2,3-Dimethoxy-9-acridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 4101-30-8
2-amino-4,5-dimethoxyacetophenone

: 98-80-6
phenylboronic acid

: 86640-16-6
2,3-dimethoxyacridin-9(10H)-one

Guidance literature:: With pyridine; oxygen; copper(II) nitrate; In dimethyl sulfoxide; at 130 ℃; for 26h; under 760.051 Torr;
DOI:10.1021/acs.orglett.8b00957

Reference yield: 64.0%

: 3972-65-4
1-bromo-4-tert-butylbenzene

: 86640-16-6
2,3-dimethoxyacridin-9(10H)-one

: N-(4-tert-butylphenyl)-2,3-dimethoxyacridone

Guidance literature:: With copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; potassium carbonate; In N,N-dimethyl-formamide; at 160 ℃; for 48h;
DOI:10.1039/d1ob01249e

Reference yield:

: 86640-16-6
2,3-dimethoxyacridin-9(10H)-one

: N-(4-tert-butylphenyl)-3-methoxyacridine-1,2,9-trione

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; potassium carbonate; 2,2,6,6-tetramethylheptane-3,5-dione / N,N-dimethyl-formamide / 48 h / 160 °C

2: ammonium cerium (IV) nitrate / dichloromethane; acetonitrile; water / 0.25 h / 20 °C

With copper(l) iodide; ammonium cerium (IV) nitrate; 2,2,6,6-tetramethylheptane-3,5-dione; potassium carbonate; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/d1ob01249e