Di-tert-butyl bicyclo[4.1.0]heptane-7,7-dicarboxylate

Base Information

Chemical Name:Di-tert-butyl bicyclo[4.1.0]heptane-7,7-dicarboxylate
CAS No.:35207-83-1
Molecular Formula:C₁₇H₂₈O₄
Molecular Weight:296.407
Hs Code.:
NSC Number:138648
DSSTox Substance ID:DTXSID70300746

Synonyms:35207-83-1;di-tert-butyl bicyclo[4.1.0]heptane-7,7-dicarboxylate;NSC138648;DTXSID70300746;NSC-138648

Suppliers and Price of Di-tert-butyl bicyclo[4.1.0]heptane-7,7-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Di-tert-butyl bicyclo[4.1.0]heptane-7,7-dicarboxylate

Chemical Property:

Vapor Pressure:0.000156mmHg at 25°C
Boiling Point:331.4°C at 760 mmHg
Flash Point:150.6°C
Density:1.066g/cm³
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:296.19875937
Heavy Atom Count:21
Complexity:397

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)C1(C2C1CCCC2)C(=O)OC(C)(C)C

Technology Process of Di-tert-butyl bicyclo[4.1.0]heptane-7,7-dicarboxylate

There total 2 articles about Di-tert-butyl bicyclo[4.1.0]heptane-7,7-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 541-16-2
t-butyl malonate

: 35207-83-1
7,7-Di-t-butoxycarbonylnorcaran

Guidance literature:: Multi-step reaction with 2 steps

1: TsN₃, Et₃N / benzene / 672 h / Ambient temperature

2: Cu catalyst / Heating

With 4-toluenesulfonyl azide; triethylamine; Cu catalyst; In benzene;
DOI:10.1016/0040-4020(76)80080-4 DOI:10.1055/s-1971-21790