Technology Process of Tetraethyl-bis(aminoethanethiol)
There total 4 articles about Tetraethyl-bis(aminoethanethiol) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diphenyl ditelluride; phosphoric acid;
In
methanol;
for 10h;
Yield given;
Heating;
DOI:10.1021/jo00102a028
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 70 percent / S2Cl2 / CCl4 / 1.) 60-65 deg C, 2 h, 2.) 50 deg C, 16 h
2: ethanol / 4 h / Heating
3: NaBH4 / ethanol / 2 h / Ambient temperature
4: (PhTe)2, 50percent aq. H3PO4 / methanol / 10 h / Heating
With
disulfur dichloride; sodium tetrahydroborate; diphenyl ditelluride; phosphoric acid;
In
methanol; tetrachloromethane; ethanol;
DOI:10.1021/jo00102a028
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ethanol / 4 h / Heating
2: NaBH4 / ethanol / 2 h / Ambient temperature
3: (PhTe)2, 50percent aq. H3PO4 / methanol / 10 h / Heating
With
sodium tetrahydroborate; diphenyl ditelluride; phosphoric acid;
In
methanol; ethanol;
DOI:10.1021/jo00102a028
