4-Tributylstannylbenzonitrile

Base Information

Chemical Name:4-Tributylstannylbenzonitrile
CAS No.:79048-30-9
Molecular Formula:C19H31NSn
Molecular Weight:392.172
Hs Code.:
DSSTox Substance ID:DTXSID10438754

Synonyms:4-tributylstannylbenzonitrile;Benzonitrile, 4-(tributylstannyl)-;79048-30-9;SCHEMBL1453582;tributyl(4-cyanophenyl)stannane;DTXSID10438754;KYZSAPVESUHUGX-UHFFFAOYSA-N

Suppliers and Price of 4-Tributylstannylbenzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 4-Tributylstannylbenzonitrile

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:10
Exact Mass:393.147853
Heavy Atom Count:21
Complexity:287

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)C1=CC=C(C=C1)C#N

Technology Process of 4-Tributylstannylbenzonitrile

There total 9 articles about 4-Tributylstannylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 623-00-7
4-bromobenzenecarbonitrile

: 1461-22-9
tributyltin chloride

: 79048-30-9
tributyl(4-cyanophenyl)stannane

Guidance literature:: With trifluoroacetic acid; cobalt(II) bromide; zinc; In acetonitrile; CoBr2 and Zn dust activated with CF3CO2H reacted for 5 min with allyl chloride in MeCN, aryl halide and tributylstannyl chloride added simultaneously in MeCN at room temp., stirred for 1 h at 50°C;
DOI:10.1039/b417326k

Reference yield: 85.0%

: 3058-39-7
4-iodobenzonitrile

: 813-19-4
bis(tri-n-butyltin)

: 79048-30-9
tributyl(4-cyanophenyl)stannane

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; byproducts: (C4H9)3SnI; soln. of Bu3SnSnBu3, Pd(PPh3)4, aryl iodide in toluene heated to 60°C for 72 h under Ar; evapd., washed with aq. KF, extd. (C6H6), dried over Na2SO4, chromd. (SiO2, hexane); elem. anal.;
DOI:10.1246/bcsj.56.3855