Stannane, tributyl(2-nitrophenyl)-

Base Information

Chemical Name:Stannane, tributyl(2-nitrophenyl)-
CAS No.:79062-30-9
Molecular Formula:C18H31NO2Sn
Molecular Weight:412.16
Hs Code.:
DSSTox Substance ID:DTXSID10462852

Synonyms:Stannane, tributyl(2-nitrophenyl)-;79062-30-9;tributyl(2-nitrophenyl)tin;SCHEMBL225747;DTXSID10462852;XGQFUVXYDGDHKI-UHFFFAOYSA-N;1-nitro-2-(tributylstannyl)benzene

Suppliers and Price of Stannane, tributyl(2-nitrophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Stannane, tributyl(2-nitrophenyl)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:10
Exact Mass:413.137682
Heavy Atom Count:22
Complexity:295

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)C1=CC=CC=C1[N+](=O)[O-]

Technology Process of Stannane, tributyl(2-nitrophenyl)-

There total 2 articles about Stannane, tributyl(2-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 609-73-4
o-nitroiodobenzene

: 813-19-4
bis(tri-n-butyltin)

: 79062-30-9
2-(tri-n-butylstannyl)-1-nitrobenzene

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; byproducts: (C4H9)3SnI; soln. of Bu3SnSnBu3, Pd(PPh3)4, aryl iodide in toluene heated to 80°C for 72 h under Ar; evapd., washed with aq. KF, extd. (C6H6), dried over Na2SO4, chromd. (SiO2, hexane); elem. anal.;
DOI:10.1246/bcsj.56.3855

Reference yield: 67.0%

: 577-19-5
2-nitrophenyl bromide

: 813-19-4
bis(tri-n-butyltin)

: 79062-30-9
2-(tri-n-butylstannyl)-1-nitrobenzene

Guidance literature:: With palladium diacetate; tricyclohexylphosphine; In neat (no solvent); at 110 ℃; for 24h; under 760.051 Torr; Sealed tube;
DOI:10.1002/ejoc.201701463

Reference yield: 91.0%

: 1439378-42-3
C₁₇H₂₆BrNO₄Si

: 79062-30-9
2-(tri-n-butylstannyl)-1-nitrobenzene

: 1439378-43-4
C₂₃H₃₀N₂O₆Si

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1039/c3sc00056g