p-Toluic acid 1-methylhydrazide

Base Information

Chemical Name:p-Toluic acid 1-methylhydrazide
CAS No.:79129-59-2
Molecular Formula:C9H12N2O
Molecular Weight:164.207
Hs Code.:
DSSTox Substance ID:DTXSID30879524
Nikkaji Number:J1.081.976H
Wikidata:Q82861637

Synonyms:p-Toluic acid 1-methylhydrazide;79129-59-2;DTXSID30879524;AKOS006372781

Suppliers and Price of p-Toluic acid 1-methylhydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of p-Toluic acid 1-methylhydrazide

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:164.094963011
Heavy Atom Count:12
Complexity:162

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)N(C)N

Technology Process of p-Toluic acid 1-methylhydrazide

There total 1 articles about p-Toluic acid 1-methylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 874-60-2
4-methyl-benzoyl chloride

: 60-34-4
methylhydrazine

: 79129-59-2
4-Methyl-benzoic acid N-methyl-hydrazide

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1055/s-2005-869858

Reference yield: 96.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 79129-59-2
4-Methyl-benzoic acid N-methyl-hydrazide

: 863117-14-0
N'-methylene-p-tolylhydrazide

Guidance literature:: In toluene; for 18h; Heating;
DOI:10.1055/s-2005-869858

Reference yield:

: 79129-59-2
4-Methyl-benzoic acid N-methyl-hydrazide

: 118235-60-2
4-Methyl-benzoic acid N,N'-dimethyl-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / toluene / 18 h / Heating

2: 92 percent / NaCNBH₃; AcOH / methanol / 18 h / 20 °C

With sodium cyanoborohydride; acetic acid; In methanol; toluene;
DOI:10.1055/s-2005-869858