Phosphoric acid, bis(4-nitrophenyl) octadecyl ester

Base Information

• Chemical Name: Phosphoric acid, bis(4-nitrophenyl) octadecyl ester
• CAS No.: 79324-62-2
• Molecular Formula: C30H45N2O8P
• Molecular Weight: 592.67
• Mol file: 79324-62-2.mol

Synonyms:

Chemical Property of Phosphoric acid, bis(4-nitrophenyl) octadecyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphoric acid, bis(4-nitrophenyl) octadecyl ester

There total 2 articles about Phosphoric acid, bis(4-nitrophenyl) octadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + n-Octadecylphosphorsaeuredichlorid (13159-55-2) → Phosphoric acid bis-(4-nitro-phenyl) ester octadecyl ester (79324-62-2)

Guidance literature:

With triethylamine; In diethyl ether; for 24h; Ambient temperature;

DOI:10.1246/bcsj.54.2072

Reference yield:

1-octadecanol (112-92-5) → Phosphoric acid bis-(4-nitro-phenyl) ester octadecyl ester (79324-62-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 15 g / POCl₃, Et₃N / diethyl ether / 3 h / Ambient temperature

2: 13 percent / Et₃N / diethyl ether / 24 h / Ambient temperature

With triethylamine; trichlorophosphate; In diethyl ether;

DOI:10.1246/bcsj.54.2072

Reference yield:

Phosphoric acid bis-(4-nitro-phenyl) ester octadecyl ester (79324-62-2) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0)

Guidance literature:

With cetyltrimethylammonim bromide; N-methyloctadecanehydroxamic acid; In water; at 30 ℃; Rate constant; Kinetics; Mechanism; pH 8.7; also in the presence of var. dialkylammonium bilayer membranes;

DOI:10.1246/bcsj.54.2072

upstream raw materials:

4-nitro-phenol

n-Octadecylphosphorsaeuredichlorid

1-octadecanol

Downstream raw materials:

4-nitro-phenol