Ethyl 2-[(E)-(4-bromophenyl)diazenyl]-3-oxobutanoate

Base Information

Chemical Name:Ethyl 2-[(E)-(4-bromophenyl)diazenyl]-3-oxobutanoate
CAS No.:79326-44-6
Molecular Formula:C12H13BrN2O3
Molecular Weight:313.151
Hs Code.:
DSSTox Substance ID:DTXSID20515227

Synonyms:79326-44-6;Ethyl 2-[(E)-(4-bromophenyl)diazenyl]-3-oxobutanoate;DTXSID20515227

Suppliers and Price of Ethyl 2-[(E)-(4-bromophenyl)diazenyl]-3-oxobutanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethyl 2-[(E)-(4-bromophenyl)diazenyl]-3-oxobutanoate

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:312.01095
Heavy Atom Count:18
Complexity:325

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(C(=O)C)N=NC1=CC=C(C=C1)Br

Technology Process of Ethyl 2-[(E)-(4-bromophenyl)diazenyl]-3-oxobutanoate

There total 3 articles about Ethyl 2-[(E)-(4-bromophenyl)diazenyl]-3-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 2028-85-5
(4-bromophenyl)diazonium chloride

: 141-97-9
ethyl acetoacetate

: 79326-44-6
ethyl-α-(4-bromo phenylazo)acetoacetate

Guidance literature:: With sodium acetate; In ethanol; for 0.166667h;

Reference yield:

: 141-97-9
ethyl acetoacetate

: 106-40-1
4-bromo-aniline

: 79326-44-6
ethyl-α-(4-bromo phenylazo)acetoacetate

Guidance literature:: 4-bromo-aniline; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 0.0833333h;

ethyl acetoacetate; With ammonium acetate; In ethanol; water;
DOI:10.3390/molecules23071543