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106-40-1 Usage

Reactivity Profile

Vapor may form highly reactive mixtures in air.

Purification Methods

Crystallise the aniline (with appreciable loss) from aqueous EtOH. The benzoyl derivative has m 204o (from EtOH). [Beilstein 12 IV 1497.]

General Description

Brown solid with a sweet odor.

Uses

4-Bromoaniline is a brominated aniline used as a building block in the preparation or pharmaceutial and organic compounds.

Uses

In preparation of azo dyes; condensed with formaldehyde in preparation of dihydroquinazolines.

Air & Water Reactions

4-Bromoaniline is sensitive to prolonged exposure to air. Vapor may form highly reactive mixtures in air . Insoluble in water.

Fire Hazard

Flash point data are not available for 4-Bromoaniline, but 4-Bromoaniline is probably combustible.

Chemical Properties

brown crystals

Synthesis Reference(s)

The Journal of Organic Chemistry, 40, p. 1867, 1975 DOI: 10.1021/jo00900a053Synthetic Communications, 19, p. 3047, 1989 DOI: 10.1080/00397918908052699
InChI:InChI=1/C6H6BrN.ClH/c7-5-1-3-6(8)4-2-5;/h1-4H,8H2;1H

106-40-1 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A15126)  4-Bromoaniline, 98+%    106-40-1 50g 221.0CNY Detail
Alfa Aesar (A15126)  4-Bromoaniline, 98+%    106-40-1 250g 770.0CNY Detail
Alfa Aesar (A15126)  4-Bromoaniline, 98+%    106-40-1 1000g 1615.0CNY Detail

106-40-1SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 4-Bromoaniline

1.2 Other means of identification

Product number -
Other names para bromo aniline

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:106-40-1 SDS

106-40-1Synthetic route

para-nitrophenyl bromide
586-78-7

para-nitrophenyl bromide

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With copper(I) chloride; potassium borohydride In methanol for 0.166667h; Ambient temperature;100%
With sodium tetrahydroborate In methanol at 60℃; for 3h; Sealed tube;100%
With water; oxalic acid; titanium(IV) oxide for 3h; Wavelength; Irradiation; Inert atmosphere; Sealed tube; Green chemistry; chemoselective reaction;100%
N-(4-bromophenyl)-1-tert-butyl-1,1-dimethylsilanamine
108613-06-5

N-(4-bromophenyl)-1-tert-butyl-1,1-dimethylsilanamine

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With silica gel In ethanol; water at 20℃; for 2h;100%
aniline
62-53-3

aniline

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With oxygen; sodium bromide In dibutyl ether at 45℃; under 760.051 Torr; for 5h; Schlenk technique;99%
With N-Bromosuccinimide at 20℃; for 0.166667h; regioselective reaction;98%
With 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one for 0.0138889h; microwave irradiation;95%
1-azido-4-bromobenzene
2101-88-4

1-azido-4-bromobenzene

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With iron(III) oxide; hydrazine hydrate In water at 120℃; for 2h; Inert atmosphere;98%
With chloro-trimethyl-silane; sodium iodide In acetonitrile for 0.166667h; Ambient temperature;97%
With borohydride supported on an ion exchange resin In methanol for 4h; Product distribution; Heating; other aryl azides and arylsulfonyl azides; var. temp. and times;96%
4-bromoacetanilide
103-88-8

4-bromoacetanilide

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With 40% potassium fluoride/alumina at 85℃; for 0.0666667h; Microwave irradiation; Neat (no solvent);97%
With ammonium bromide; ethylenediamine at 70℃; for 5h; Microwave irradiation; Inert atmosphere; neat (no solvent);96%
With [RuCl2(2-(diphenylphosphino)-N-((6-((diphenylphosphino)methyl)pyridin-2-yl)methyl)ethan-1-amine)]; potassium tert-butylate; hydrogen In tetrahydrofuran at 100℃; under 37503.8 Torr; for 20h; Catalytic behavior; Autoclave; chemoselective reaction;95%
para-nitrophenyl bromide
586-78-7

para-nitrophenyl bromide

A

aniline
62-53-3

aniline

B

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With platinum on carbon; hydrogen In methanol at 25℃; under 1500.15 Torr; for 24h; Catalytic behavior; Solvent; Temperature; Reagent/catalyst; Pressure;A 90%
B 5%
With isopropyl alcohol; sodium hydroxide for 12h; Inert atmosphere; Reflux; chemoselective reaction;A n/a
B 84%
With hydrogen In methanol at 30℃; under 22502.3 Torr; Reagent/catalyst;A n/a
B 83%
1,4-bromoiodobenzene
589-87-7

1,4-bromoiodobenzene

A

1-azido-4-bromobenzene
2101-88-4

1-azido-4-bromobenzene

B

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With sodium azide; copper; diisopropylamine; ascorbic acid In dimethyl sulfoxide at 80℃; for 14h;A 88%
B 7%
aniline
62-53-3

aniline

A

4-bromo-aniline
106-40-1

4-bromo-aniline

B

2-bromoaniline
615-36-1

2-bromoaniline

Conditions
ConditionsYield
With dihydrogen peroxide; potassium bromide In water; acetonitrileA 87%
B 12%
With pyridinium hydrobromide perbromide In tetrahydrofuran for 0.25h; Product distribution; other aromatic amines;A 84%
B n/a
With N-Bromosuccinimide; silver hexafluoroantimonate; 1-methylthiotriptycene In 1,2-dichloro-ethane at 20℃; for 1h; Inert atmosphere; Schlenk technique; Overall yield = 95 percentSpectr.;A 76%
B n/a
(E)-N-(4-bromophenyl)-1-(p-tolyl)methanimine
124397-40-6

(E)-N-(4-bromophenyl)-1-(p-tolyl)methanimine

malononitrile
109-77-3

malononitrile

A

2-(4-methylbenzylidene)malononitrile
2826-25-7

2-(4-methylbenzylidene)malononitrile

B

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With sodium dodecyl-sulfate In water at 25 - 30℃; for 0.2h;A 87%
B n/a
(4-bromo-phenyl)-carbamic acid 2,2,2-trichloro-ethyl ester

(4-bromo-phenyl)-carbamic acid 2,2,2-trichloro-ethyl ester

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With indium; ammonium chloride In ethanol for 2.5h; Heating;86%
1,2-bis(4-bromophenyl)diazene
1601-98-5

1,2-bis(4-bromophenyl)diazene

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With perchloric acid In isopropyl alcohol; acetonitrile at 25℃; for 0.583333h; pH=2; Inert atmosphere; Irradiation;86%
2-(4-bromophenoxy)propanamide
360791-98-6

2-(4-bromophenoxy)propanamide

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With potassium hydroxide In dimethyl sulfoxide at 140℃; for 3h; Green chemistry;86%
With potassium hydroxide at 140℃;126.5 mg
methyl N-(4-bromophenyl)carbamate
25203-36-5

methyl N-(4-bromophenyl)carbamate

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With sodium hydrogen telluride In N,N-dimethyl-formamide at 70 - 75℃; for 5h;85%
With water; hydrogen cation at 99.9℃; Rate constant;
indole
120-72-9

indole

2-phenyl-1,2,3,4-tetrahydroisoquinoline
3340-78-1

2-phenyl-1,2,3,4-tetrahydroisoquinoline

para-nitrophenyl bromide
586-78-7

para-nitrophenyl bromide

A

1-(1H-indol-3-yl)-2-phenyl-1, 2, 3, 4-tetrahydroisoquinoline

1-(1H-indol-3-yl)-2-phenyl-1, 2, 3, 4-tetrahydroisoquinoline

B

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With Co(dmgH)2Cl2; Eosin Y In water; acetonitrile at 20℃; for 48h; Inert atmosphere; Irradiation; Sealed tube;A 85%
B 94 %Spectr.
aniline
62-53-3

aniline

A

2,4-dibromo-aniline
615-57-6

2,4-dibromo-aniline

B

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With tetra-N-butylammonium tribromide In chloroform for 0.05h;A 14%
B 84%
With tetra-N-butylammonium tribromide In chloroform at 20℃; for 0.05h; Product distribution; substituted anilines, 2-aminopyridine, other solvents, other reaction time, other reagent: tetraphenylphosphonium tribromide;A 16%
B 82%
With tetra-N-butylammonium tribromide In chloroform at 20℃; for 0.05h; other reagent: tetraphenylphosphonium tribromide;A 16%
B 82%
N,N',N''-tris(p-bromophenyl)phosphorous triamide

N,N',N''-tris(p-bromophenyl)phosphorous triamide

A

2,4-bis(p-bromoanilino)-1,3-bis(p-bromophenyl)-1,3,2,4-diazadiphosphetidine

2,4-bis(p-bromoanilino)-1,3-bis(p-bromophenyl)-1,3,2,4-diazadiphosphetidine

B

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
In xylene for 2h; Heating;A 60.5%
B 83.5%
para-nitrophenyl bromide
586-78-7

para-nitrophenyl bromide

A

1,2-bis(4-bromophenyl)diazene
1601-98-5

1,2-bis(4-bromophenyl)diazene

B

4-bromo-aniline
106-40-1

4-bromo-aniline

C

4,4'-dibromoazoxybenzene
1215-42-5, 21650-67-9, 125367-64-8

4,4'-dibromoazoxybenzene

Conditions
ConditionsYield
With hydrazine hydrate; nickel(II) nitrate; zinc In tert-butyl alcohol for 0.333333h; Heating;A 6 % Chromat.
B 8%
C 82%
With hydrazine hydrate; nickel(II) nitrate; zinc In ethanol for 3h; Heating;A 13%
B 5%
C 79%
para-nitrophenyl bromide
586-78-7

para-nitrophenyl bromide

A

4-bromo-aniline
106-40-1

4-bromo-aniline

B

p,p'-diaminobiphenyl
92-87-5

p,p'-diaminobiphenyl

Conditions
ConditionsYield
With hydrazine hydrate In ethanol at 70℃; for 4h; chemoselective reaction;A 82%
B 7%
benzyl (4-bromophenyl)carbamate
92159-87-0

benzyl (4-bromophenyl)carbamate

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With methanol; sodium tetrahydroborate; nickel(II) chloride hexahydrate at 20℃; for 0.25h; chemoselective reaction;81%
1-(4-bromophenyl)ethanol
5391-88-8

1-(4-bromophenyl)ethanol

4-bromo-aniline
106-40-1

4-bromo-aniline

Conditions
ConditionsYield
With sodium azide; methanesulfonic acid; trifluoroacetic acid In hexane at 40℃; for 10h;81%
With sodium azide; methanesulfonic acid; trifluoroacetic acid In hexane at 40℃; for 4h; Sealed tube;78%
4,7-dichloroquinoline
86-98-6

4,7-dichloroquinoline

4-bromo-aniline
106-40-1

4-bromo-aniline

N-(4-bromophenyl)-7-chloroquinolin-4-amine

N-(4-bromophenyl)-7-chloroquinolin-4-amine

Conditions
ConditionsYield
In ethanol for 24h; Reflux;100%
for 0.166667h; microwave irradiation;95%
With ethanol
4-hydroxy-benzaldehyde
123-08-0

4-hydroxy-benzaldehyde

4-bromo-aniline
106-40-1

4-bromo-aniline

4-hydroxybenzylidene-4'-bromoaniline
3382-65-8

4-hydroxybenzylidene-4'-bromoaniline

Conditions
ConditionsYield
for 24h; Ambient temperature;100%
In methanol at 20℃;90%
With sulfuric acid In neat (no solvent) Microwave irradiation; Sealed tube; Green chemistry;87%
methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

4-bromo-aniline
106-40-1

4-bromo-aniline

N-(4-bromophenyl)methanesulfonamide
4284-50-8

N-(4-bromophenyl)methanesulfonamide

Conditions
ConditionsYield
Stage #1: methanesulfonyl chloride; 4-bromo-aniline With triethylamine In dichloromethane at 0 - 20℃; for 3.08333h;
Stage #2: With methanol; ammonia; water In tetrahydrofuran at 20℃; for 16h;
100%
Stage #1: methanesulfonyl chloride; 4-bromo-aniline With triethylamine In dichloromethane at 0 - 20℃; for 3.08333h;
Stage #2: With ammonia; water In tetrahydrofuran; methanol at 20℃; for 16h;
100%
With pyridine In dichloromethane at 0 - 20℃; for 12h;98%
butyryl chloride
141-75-3

butyryl chloride

4-bromo-aniline
106-40-1

4-bromo-aniline

N-(4-bromophenyl)butanamide
119199-11-0

N-(4-bromophenyl)butanamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 5 - 20℃;100%
With triethylamine In chloroform at 20℃; for 0.0222222h; Flow reactor;82%
Benzoyl isothiocyanate
532-55-8

Benzoyl isothiocyanate

4-bromo-aniline
106-40-1

4-bromo-aniline

1-benzoyl-3-(4-bromophenyl)thiourea
19249-89-9

1-benzoyl-3-(4-bromophenyl)thiourea

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 1.2h;100%
In acetone82%
at 75℃; for 2h; Reflux;72%
p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

4-bromo-aniline
106-40-1

4-bromo-aniline

N-(4-bromophenyl)-4-methylbenzenesulfonamide
32857-48-0

N-(4-bromophenyl)-4-methylbenzenesulfonamide

Conditions
ConditionsYield
With pyridine In dichloromethane for 2h; Inert atmosphere;100%
With triethylamine In dichloromethane at 4℃;100%
With pyridine In dichloromethane at 20℃; for 16h;99%
formic acid
64-18-6

formic acid

4-bromo-aniline
106-40-1

4-bromo-aniline

N-(4-bromophenyl)formamide
2617-78-9

N-(4-bromophenyl)formamide

Conditions
ConditionsYield
In toluene Reflux;100%
With sodium formate at 20℃; for 2.75h; Neat (no solvent);99%
With zinc(II) oxide at 70℃; for 0.333333h;98%
4-bromo-aniline
106-40-1

4-bromo-aniline

4-bromonitrosobenzene
3623-23-2

4-bromonitrosobenzene

Conditions
ConditionsYield
With Oxone In dichloromethane; water at 20℃; for 4h;100%
With oxone||potassium monopersulfate triple salt In dichloromethane; water at 20℃;100%
With dihydrogen peroxide In methanol; water at 20℃; for 2h; Catalytic behavior; Sealed tube; chemoselective reaction;94%
acetic anhydride
108-24-7

acetic anhydride

4-bromo-aniline
106-40-1

4-bromo-aniline

4-bromoacetanilide
103-88-8

4-bromoacetanilide

Conditions
ConditionsYield
With cadmium(II) oxide at 80℃; for 0.166667h; Neat (no solvent); Microwave irradiation;100%
In dichloromethane at 20℃; Inert atmosphere;100%
In dichloromethane at 0 - 20℃; Inert atmosphere;100%
3,4-dimethoxy-benzaldehyde
120-14-9

3,4-dimethoxy-benzaldehyde

4-bromo-aniline
106-40-1

4-bromo-aniline

3,4-dimethoxybenzal-4-bromoaniline
82363-27-7

3,4-dimethoxybenzal-4-bromoaniline

Conditions
ConditionsYield
In toluene Heating;100%
In methanol at 20℃;76%
4-bromo-aniline
106-40-1

4-bromo-aniline

1,4-bromoiodobenzene
589-87-7

1,4-bromoiodobenzene

Conditions
ConditionsYield
Stage #1: 4-bromo-aniline With hydrogenchloride; sodium nitrite In water at 0 - 5℃; for 0.5h; Inert atmosphere;
Stage #2: With potassium iodide In ethyl acetate for 0.5h;
100%
With sulfuric acid; potassium iodide; sodium nitrite In water at -5 - 60℃; Inert atmosphere;92%
Stage #1: 4-bromo-aniline With sulfuric acid; silica gel; sodium nitrite at 20℃; grinding; Neat (no solvent);
Stage #2: With water at 20℃; grinding; Neat (no solvent);
Stage #3: With potassium iodide at 20℃; for 0.166667h; Sandmeyer reaction; grinding; Neat (no solvent);
87%
methyl thioisocyanate
556-61-6

methyl thioisocyanate

4-bromo-aniline
106-40-1

4-bromo-aniline

1-(4-bromophenyl)-3-methyl-thiourea
61449-55-6

1-(4-bromophenyl)-3-methyl-thiourea

Conditions
ConditionsYield
at 20℃; for 24h; Addition; solid-phase reaction;100%
In ethanol for 1h; Heating;
4-bromo-aniline
106-40-1

4-bromo-aniline

phenylboronic acid
98-80-6

phenylboronic acid

4-Aminobiphenyl
92-67-1

4-Aminobiphenyl

Conditions
ConditionsYield
With potassium carbonate In methanol at 75℃; for 0.0833333h; Catalytic behavior; Suzuki-Miyaura Coupling; Microwave irradiation;100%
With C22H21Cl4N4O3Pd2S(1-)*C16H36N(1+); potassium carbonate In water at 75℃; for 2h; Reagent/catalyst; Suzuki Coupling; Schlenk technique;99%
With sodium carbonate; palladium In ethanol; water at 20 - 83℃; for 0.366667h; Concentration; Suzuki Coupling; Microwave irradiation;99%
4-bromo-aniline
106-40-1

4-bromo-aniline

propiononitrile
107-12-0

propiononitrile

N-(4-bromo-phenyl)-propionamidine

N-(4-bromo-phenyl)-propionamidine

Conditions
ConditionsYield
With aluminium trichloride In toluene at 107℃; for 1.5h;100%
ortho-nitrofluorobenzene
1493-27-2

ortho-nitrofluorobenzene

4-bromo-aniline
106-40-1

4-bromo-aniline

4-bromo-N-(2-nitrophenyl)benzenamine
58476-59-8

4-bromo-N-(2-nitrophenyl)benzenamine

Conditions
ConditionsYield
In dimethyl sulfoxide at 100℃; for 48h; Inert atmosphere; Schlenk technique;100%
With potassium fluoride at 170 - 180℃; for 30h;92%
With potassium fluoride at 150℃; for 18h; Inert atmosphere;90%
4-bromo-aniline
106-40-1

4-bromo-aniline

4,6-dimethyl-1H-pyrazolo[3,4-b]pyridine-3-diazonium nitrate

4,6-dimethyl-1H-pyrazolo[3,4-b]pyridine-3-diazonium nitrate

3-(4-bromophenyl)-1-(4,6-dimethyl-1H-pyrazolo[3,4-b]pyridine-3-yl)triazene

3-(4-bromophenyl)-1-(4,6-dimethyl-1H-pyrazolo[3,4-b]pyridine-3-yl)triazene

Conditions
ConditionsYield
With trimethylamine at 20℃; under 375.03 Torr; for 12h;100%
3-hydroxypyridine-4-carboxaldehyde
1849-54-3

3-hydroxypyridine-4-carboxaldehyde

4-bromo-aniline
106-40-1

4-bromo-aniline

4-{[(E)-4-Bromo-phenylimino]-methyl}-pyridin-3-ol

4-{[(E)-4-Bromo-phenylimino]-methyl}-pyridin-3-ol

Conditions
ConditionsYield
In toluene Heating;100%
In toluene for 5h; Heating;82%
3-chloro-3-oxopropanoic acid methyl ester
37517-81-0

3-chloro-3-oxopropanoic acid methyl ester

4-bromo-aniline
106-40-1

4-bromo-aniline

methyl 3-((4-bromophenyl)amino)-3-oxopropanoate
669000-20-8

methyl 3-((4-bromophenyl)amino)-3-oxopropanoate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃;100%
Stage #1: 4-bromo-aniline With triethylamine In ethyl acetate at 10℃;
Stage #2: 3-chloro-3-oxopropanoic acid methyl ester at 17℃; for 0.75h;
122.75 g
N-(2-ethylhexyl)-1,7-(3',5'-di-tert-butoxyphenoxy)perylene-3,4-dicarboxyanydride-9,10-dicarboxyimide

N-(2-ethylhexyl)-1,7-(3',5'-di-tert-butoxyphenoxy)perylene-3,4-dicarboxyanydride-9,10-dicarboxyimide

4-bromo-aniline
106-40-1

4-bromo-aniline

C66H69BrN2O6

C66H69BrN2O6

Conditions
ConditionsYield
With 1H-imidazole In toluene for 3h; Reflux;100%
4-bromo-aniline
106-40-1

4-bromo-aniline

2,3-dichlorobenzeneboronic acid
151169-74-3

2,3-dichlorobenzeneboronic acid

2',3'-dichlorobiphenyl-4-amine
1148126-14-0

2',3'-dichlorobiphenyl-4-amine

Conditions
ConditionsYield
With palladium diacetate; potassium carbonate; triphenylphosphine In toluene for 24h; Suzuki coupling; Inert atmosphere; Reflux;100%
dimethyl acetylenedicarboxylate
762-42-5

dimethyl acetylenedicarboxylate

4-bromo-aniline
106-40-1

4-bromo-aniline

dimethyl 2-(4-bromophenylamino)maleate
106509-83-5

dimethyl 2-(4-bromophenylamino)maleate

Conditions
ConditionsYield
at 20℃; for 0.133333h; Milling; Inert atmosphere;100%
In methanol at 70℃; for 24h; Michael addition;79%
1-(2,5-dimethyl-1H-pyrrol-1-yl)prop-2-en-1-one
1258500-12-7

1-(2,5-dimethyl-1H-pyrrol-1-yl)prop-2-en-1-one

4-bromo-aniline
106-40-1

4-bromo-aniline

N-(3-(2,5-dimethyl-1H-pyrrol-1-yl)-3-oxoprop-1-yl)-4-bromoaniline
1258500-19-4

N-(3-(2,5-dimethyl-1H-pyrrol-1-yl)-3-oxoprop-1-yl)-4-bromoaniline

Conditions
ConditionsYield
In water at 50℃; for 24h; Michael condensation;100%
bis(trichloromethyl) carbonate
32315-10-9

bis(trichloromethyl) carbonate

4-bromo-aniline
106-40-1

4-bromo-aniline

4-bromophenyl isocyanate
2493-02-9

4-bromophenyl isocyanate

Conditions
ConditionsYield
With triethylamine In dichloromethane100%
Stage #1: bis(trichloromethyl) carbonate; 4-bromo-aniline In dichloromethane at 20℃; for 0.5h;
Stage #2: With triethylamine In dichloromethane at -35 - 20℃; for 2h;
93%
With triethylamine In toluene for 7h; Reflux; Cooling with ice;72%
(E)-3-phenylpropenal
14371-10-9

(E)-3-phenylpropenal

4-bromo-aniline
106-40-1

4-bromo-aniline

(1E,2E)-N-(4-bromophenyl)-3-phenylprop-2-en-1-imine

(1E,2E)-N-(4-bromophenyl)-3-phenylprop-2-en-1-imine

Conditions
ConditionsYield
In neat (no solvent) for 0.25h;100%
4-bromo-aniline
106-40-1

4-bromo-aniline

propiononitrile
107-12-0

propiononitrile

C9H11BrN2

C9H11BrN2

Conditions
ConditionsYield
With aluminum (III) chloride In toluene at 100℃; for 0.0833333h;100%
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