Boroxin, tris(3-methoxyphenyl)-

Base Information

• Chemical Name: Boroxin, tris(3-methoxyphenyl)-
• CAS No.: 79421-99-1
• Molecular Formula: C21H21B3O6
• Molecular Weight: 401.827
• Mol file: 79421-99-1.mol

Synonyms:

Chemical Property of Boroxin, tris(3-methoxyphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Boroxin, tris(3-methoxyphenyl)-

There total 4 articles about Boroxin, tris(3-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxyphenylboronic acid (10365-98-7,1107579-37-2) → tris(3-methoxyphenyl)-1,3,5,2,4,6-trioxatriborinane (79421-99-1)

Guidance literature:

at 105 ℃;

Reference yield:

C7H9B3O4 → tris(3-methoxyphenyl)-1,3,5,2,4,6-trioxatriborinane (79421-99-1)

Guidance literature:

In toluene; for 1.5h; Reflux; Inert atmosphere;

DOI:10.1021/ol301912a

Reference yield:

triisobutyl borate (13195-76-1) + (3-methoxyphenyl)magnesium bromide (36282-40-3) → tris(3-methoxyphenyl)-1,3,5,2,4,6-trioxatriborinane (79421-99-1)

Guidance literature:

With water; byproducts: H2O; dehydration at 105°C and over H2SO4;;

upstream raw materials:

3-methoxyphenylboronic acid

(3-methoxyphenyl)magnesium bromide

triisobutyl borate

Downstream raw materials:

1-fluoro-3-methoxybenzene

methoxybenzene

(R)-N-[(3-methoxyphenyl)phenylmethyl]-4-nitrobenzenesulfonamide

2-(3-methoxyphenyl)-but-3-en-1-ol