2,4-dinitrophenyl diphenylcarbamodithioate

Base Information

• Chemical Name: 2,4-dinitrophenyl diphenylcarbamodithioate
• CAS No.: 25675-98-3
• Molecular Formula: C₁₉H₁₃N₃O₄S₂
• Molecular Weight: 411.462
• Mol file: 25675-98-3.mol

Synonyms:Benzenethiol,2,4-dinitro-, diphenyldithiocarbamate (ester) (8CI); NSC 37191

Chemical Property of 2,4-dinitrophenyl diphenylcarbamodithioate

Chemical Property:

• Vapor Pressure: 6.44E-13mmHg at 25°C
• Boiling Point: 568°Cat760mmHg
• Flash Point: 297.3°C
• Density: 1.49g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-dinitrophenyl diphenylcarbamodithioate

There total 3 articles about 2,4-dinitrophenyl diphenylcarbamodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C6H15N*C13H11NS2 (1381994-41-7) + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → 2,4-dinitrophenyl-N,N-diphenylcarbamodithioate (25675-98-3)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1021/jm3006004

Reference yield:

diphenylamine (122-39-4) → 2,4-dinitrophenyl-N,N-diphenylcarbamodithioate (25675-98-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 20 °C

2: N,N-dimethyl-formamide / 12 h / 20 °C

In N,N-dimethyl-formamide; 2: Sanger reaction;

DOI:10.1021/jm3006004

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + diphenylamine (122-39-4) + 1-chloro-2,4-dinitro-benzene (97-00-7) → 2,4-dinitrophenyl-N,N-diphenylcarbamodithioate (25675-98-3)

Guidance literature:

Multistep reaction; (i) NaOH, (ii) /BRN= 613161/;

upstream raw materials:

carbon disulfide

diphenylamine

1-chloro-2,4-dinitro-benzene

C₆H₁₅N*C₁₃H₁₁NS₂