3'-Adenylic acid, N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl )diphenylmethyl]-, 2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl ester

Base Information

Chemical Name:3'-Adenylic acid, N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl )diphenylmethyl]-, 2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl ester
CAS No.:79553-55-2
Molecular Formula:C57H57Cl2N6O11PSi
Molecular Weight:1132.08
Hs Code.:

3'-Adenylic acid,
N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl
)diphenylmethyl]-, 2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl ester

Synonyms:

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Chemical Property of 3'-Adenylic acid, N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl )diphenylmethyl]-, 2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3'-Adenylic acid, N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl )diphenylmethyl]-, 2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl ester

There total 3 articles about 3'-Adenylic acid, N-benzoyl-2'-O-[(1,1-dimethylethyl)dimethylsilyl]-5'-O-[(4-methoxyphenyl )diphenylmethyl]-, 2,5-dichlorophenyl 2-(4-nitrophenyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53676-18-9
2,5-dichlorophenyl phosphorodichloridate

: 79553-55-2
N⁶-benzoyl-2'-O<(tert-butyl)-dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 3'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate>

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / Ambient temperature

2: pyridine / 1 h / 0 °C

3: pyridine / 3 h / Ambient temperature

In pyridine;
DOI:10.1002/hlca.19810640548

Reference yield:

: 2,5-dichlorophenylphosphoro ditriazolide

: 79553-55-2
N⁶-benzoyl-2'-O<(tert-butyl)-dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 3'-<2,5-dichlorophenyl 2-(p-nitrophenyl)ethyl phosphate>

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1 h / 0 °C

2: pyridine / 3 h / Ambient temperature

In pyridine;
DOI:10.1002/hlca.19810640548