Stannanecarbodithioic acid, triphenyl-, 1-methylethyl ester

Base Information

Chemical Name:Stannanecarbodithioic acid, triphenyl-, 1-methylethyl ester
CAS No.:79634-84-7
Molecular Formula:C₂₂H₂₂S₂Sn
Molecular Weight:469.259
Hs Code.:

Synonyms:

Suppliers and Price of Stannanecarbodithioic acid, triphenyl-, 1-methylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Stannanecarbodithioic acid, triphenyl-, 1-methylethyl ester

Chemical Property:

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Stannanecarbodithioic acid, triphenyl-, 1-methylethyl ester

There total 1 articles about Stannanecarbodithioic acid, triphenyl-, 1-methylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 75-30-9
2-iodo-propane

: 75-15-0,12122-00-8
carbon disulfide

: 4167-90-2
lithium triphenylstannide

: 79634-84-7
isopropyl triphenylstannanedithiocarboxylate

Guidance literature:: In tetrahydrofuran; byproducts: LiI; to (C6H5)3SnLi in THF dropped under stirring CS2 in slight excess, colour change to red with warming, after cooling addn. of (CH3)2CHI in excess; column chromy. (silica gel/THF), solvent removed from the violet fraction, treated with ethanol, pptn., recrystd. from petroleum ether, elem. anal.;

Reference yield: 25.0%

: 79634-84-7
isopropyl triphenylstannanedithiocarboxylate

: dicarbonyl(η(5)-cyclopentadienyl)manganese(THF)

: 86921-11-1
(C₅H₅)Mn(CO)2((C₆H₅)3SnCS₂C₃H₇)

Guidance literature:: In tetrahydrofuran; react. of ester and metal carbonyl (excess) under N2 in the dark, 2h; reducing volume; chromy. (silica gel, THF/petroleum ether); evapn.; freezing in methanol; crushing; vigorously stirring up to room temp.; filtration; washing (methanol); drying; subliming off excess metal carbonyl; elem. anal.;

Reference yield: 20.0%

: 79634-84-7
isopropyl triphenylstannanedithiocarboxylate

: 36477-75-5
tungsten pentacarbonyl tetrahydrofuran

: 86921-06-4
W(CO)5((C₆H₅)3SnCS₂C₃H₇)

Guidance literature:: In tetrahydrofuran; react. of ester and metal carbonyl (excess) under N2 in the dark, 2h; reducing volume; chromy. (silica gel, THF/petroleum ether); evapn.; freezing in ethanol; crushing; vigorously stirring up to room temp.; filtration; washing (ethanol); drying; subliming off excess metal carbonyl; elem. anal.;