1H-Indole, 2-(diphenylphosphino)-3-methyl-

Base Information

Chemical Name:1H-Indole, 2-(diphenylphosphino)-3-methyl-
CAS No.:800369-69-1
Molecular Formula:C21H18NP
Molecular Weight:315.354
Hs Code.:
DSSTox Substance ID:DTXSID30479280
Nikkaji Number:J2.118.764J
Wikidata:Q82313268

Synonyms:1H-Indole, 2-(diphenylphosphino)-3-methyl-;800369-69-1;SCHEMBL14927228;DTXSID30479280;3-methylindol-2-yldiphenylphosphine

Suppliers and Price of 1H-Indole, 2-(diphenylphosphino)-3-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1H-Indole, 2-(diphenylphosphino)-3-methyl-

Chemical Property:

XLogP3:5.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:315.117686576
Heavy Atom Count:23
Complexity:354

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(NC2=CC=CC=C12)P(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 1H-Indole, 2-(diphenylphosphino)-3-methyl-

There total 6 articles about 1H-Indole, 2-(diphenylphosphino)-3-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83-34-1
3-Methylindole

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 800369-69-1
diphenyl-2-(3-methylindolyl)phosphine

Guidance literature:: 3-Methylindole; With n-butyllithium;

With carbon dioxide;

chloro-diphenylphosphine; Further stages;
DOI:10.1002/chem.200903476

Reference yield:

: 105340-00-9
1-[(N,N-dimethylamino)methyl]-3-methylindole

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 800369-69-1
diphenyl-2-(3-methylindolyl)phosphine

Guidance literature:: 1-[(N,N-dimethylamino)methyl]-3-methylindole; With n-butyllithium; In diethyl ether; at 20 ℃; for 4h; Inert atmosphere; Schlenk technique;

chloro-diphenylphosphine; In diethyl ether; at -78 - 20 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.jorganchem.2021.122175

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: Lithium 3-methylindole-1-carboxylate

: 800369-69-1
diphenyl-2-(3-methylindolyl)phosphine

Guidance literature:: Lithium 3-methylindole-1-carboxylate; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -70 ℃; for 1h; Inert atmosphere;

chloro-diphenylphosphine; In tetrahydrofuran; pentane; at -70 - 20 ℃; for 16h; Inert atmosphere;

With water; In tetrahydrofuran; pentane; Inert atmosphere;
DOI:10.1002/adsc.200800209