Cyclohexanone, O-(methylsulfonyl)oxime

Base Information Edit

Chemical Name:Cyclohexanone, O-(methylsulfonyl)oxime
CAS No.:80053-69-6
Molecular Formula:C7H13NO3S
Molecular Weight:191.251
Hs Code.:
Mol file:80053-69-6.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanone, O-(methylsulfonyl)oxime Edit

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Cyclohexanone, O-(methylsulfonyl)oxime

There total 2 articles about Cyclohexanone, O-(methylsulfonyl)oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-64-1
cyclohexanone-oxime

: 124-63-0
methanesulfonyl chloride

: 80053-69-6
cyclohexanone oxime methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at -20 ℃; for 0.666667h;
DOI:10.1021/ja00347a052

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 80053-69-6
cyclohexanone oxime methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine / isopropyl alcohol; water / 0.5 h / 0 - 20 °C

2: triethylamine / dichloromethane / 0.42 h / -22 - -15 °C / Inert atmosphere

With hydroxylamine; triethylamine; In dichloromethane; water; isopropyl alcohol;
DOI:10.1021/acs.oprd.9b00425