Technology Process of 6-nitroquinoline 1-oxide
There total 4 articles about 6-nitroquinoline 1-oxide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
benzene;
1.) 15 deg C, 15 min, 2.) 60 deg C, 10 h;
- Guidance literature:
-
Multi-step reaction with 2 steps
2: 89 percent / m-chloroperoxybenzoic acid / benzene / 1.) 15 deg C, 15 min, 2.) 60 deg C, 10 h
With
3-chloro-benzenecarboperoxoic acid;
In
benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sulfuric acid; potassium nitrate / 0 - 20 °C
1.2: Cooling with ice
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 4 h / 0 - 20 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C
With
sulfuric acid; potassium nitrate; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
DOI:10.1021/acs.jmedchem.0c00982
