Cyclo[phenylalanylprolylthreonyl-2-(1-amino-2-methylbutyl)-4-thiazolecarbonyl-2-(1-aminoethyl)-4-thiazolecarbonyl](9CI)

Base Information

• Chemical Name: Cyclo[phenylalanylprolylthreonyl-2-(1-amino-2-methylbutyl)-4-thiazolecarbonyl-2-(1-aminoethyl)-4-thiazolecarbonyl](9CI)
• CAS No.: 104928-30-5
• Molecular Formula: C33H41 N7 O6 S2
• Molecular Weight: 695.864
• Mol file: 104928-30-5.mol

Synonyms:11H-10,7:17,14-Dinitrilo-7H-pyrrolo[2,1-i][1,17,4,7,10,13,20]dithiapentaazacyclotricosine-1,4,11,18,21-pentone,2,3,5,6,12,13,19,20,23,24,25,25a-dodecahydro-3-(1-hydroxyethyl)-13-methyl-6-(1-methylpropyl)-20-(phenylmethyl)-;Preulicyclamide; Ulicyclamide, pre-

Chemical Property of Cyclo[phenylalanylprolylthreonyl-2-(1-amino-2-methylbutyl)-4-thiazolecarbonyl-2-(1-aminoethyl)-4-thiazolecarbonyl](9CI)

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Technology Process of Cyclo[phenylalanylprolylthreonyl-2-(1-amino-2-methylbutyl)-4-thiazolecarbonyl-2-(1-aminoethyl)-4-thiazolecarbonyl](9CI)

There total 2 articles about Cyclo[phenylalanylprolylthreonyl-2-(1-amino-2-methylbutyl)-4-thiazolecarbonyl-2-(1-aminoethyl)-4-thiazolecarbonyl](9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-1-[(S)-2-({2-[(R)-1-({2-[(S)-1-((2S,3S)-2-Amino-3-hydroxy-butyrylamino)-2-methyl-butyl]-thiazole-4-carbonyl}-amino)-ethyl]-thiazole-4-carbonyl}-amino)-3-phenyl-propionyl]-pyrrolidine-2-carboxylic acid (112495-89-3) → C33H41N7O6S2 (104928-30-5)

Guidance literature:

With diphenyl phosphoryl azide; triethylamine; In N,N-dimethyl-formamide; Yield given; 0-5 deg C, 3 days, room temp. 1 day;

DOI:10.1016/S0040-4039(00)96093-3

Reference yield:

(S)-1-[(S)-2-({2-[(R)-1-({2-[(S)-1-((2S,3S)-2-Benzyloxycarbonylamino-3-tert-butoxy-butyrylamino)-2-methyl-butyl]-thiazole-4-carbonyl}-amino)-ethyl]-thiazole-4-carbonyl}-amino)-3-phenyl-propionyl]-pyrrolidine-2-carboxylic acid methyl ester (112495-88-2) → C33H41N7O6S2 (104928-30-5)

Guidance literature:

Multi-step reaction with 2 steps

2: diphenyl phosphoroazidate, NEt₃ / dimethylformamide / 0-5 deg C, 3 days, room temp. 1 day

With diphenyl phosphoryl azide; triethylamine; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)96093-3

Reference yield: 100.0%

C33H41N7O6S2 (104928-30-5) → ulicyclamide (74839-81-9)

Guidance literature:

With thionyl chloride; at 0 - 5 ℃; for 30h;

DOI:10.1016/S0040-4039(00)96093-3

upstream raw materials:

(S)-1-[(S)-2-({2-[(R)-1-({2-[(S)-1-((2S,3S)-2-Amino-3-hydroxy-butyrylamino)-2-methyl-butyl]-thiazole-4-carbonyl}-amino)-ethyl]-thiazole-4-carbonyl}-amino)-3-phenyl-propionyl]-pyrrolidine-2-carboxylic acid

(S)-1-[(S)-2-({2-[(R)-1-({2-[(S)-1-((2S,3S)-2-Benzyloxycarbonylamino-3-tert-butoxy-butyrylamino)-2-methyl-butyl]-thiazole-4-carbonyl}-amino)-ethyl]-thiazole-4-carbonyl}-amino)-3-phenyl-propionyl]-pyrrolidine-2-carboxylic acid methyl ester

Downstream raw materials:

ulicyclamide

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