N,N,N',N'-Tetramethyl-1-(phenylphosphanylidene)methanediamine

Base Information

Chemical Name:N,N,N',N'-Tetramethyl-1-(phenylphosphanylidene)methanediamine
CAS No.:80592-10-5
Molecular Formula:C11H17N2P
Molecular Weight:208.243
Hs Code.:
DSSTox Substance ID:DTXSID30512025
Nikkaji Number:J2.119.976A
Wikidata:Q82371098

Synonyms:80592-10-5;DTXSID30512025;N,N,N',N'-Tetramethyl-1-(phenylphosphanylidene)methanediamine

Suppliers and Price of N,N,N',N'-Tetramethyl-1-(phenylphosphanylidene)methanediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N,N,N',N'-Tetramethyl-1-(phenylphosphanylidene)methanediamine

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:208.112935548
Heavy Atom Count:14
Complexity:184

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C(=PC1=CC=CC=C1)N(C)C

Technology Process of N,N,N',N'-Tetramethyl-1-(phenylphosphanylidene)methanediamine

There total 1 articles about N,N,N',N'-Tetramethyl-1-(phenylphosphanylidene)methanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C-Ethoxy-N,N,N',N'-tetramethyl-C-phenylphosphanyl-methanediamine

: 64-17-5
ethanol

: 80592-10-5
phenylphosphine

Guidance literature:: In diethyl ether; at -40 ℃; Yield given;

Reference yield: 66.0%

: 67784-65-0
chlorotris(trimethyl phosphite)copper(I)

: 80592-10-5
phenylphosphine

: [Cu3Cl3(μ-P(Ph)C(NMe2)2)3]

Guidance literature:: In tetrahydrofuran; pentane; all manipulations under N2 atm.; soln. of org. compd. in pentane added dropwise at 0°C slowly to soln. of Cu compd. in THF, stirred at room temp. for 16 h; filtered, recrystd. from THF; elem. anal.;
DOI:10.1002/zaac.200400233

Reference yield: 50.0%

: 80592-10-5
phenylphosphine

: 525-06-4
diphenyl ketene

: 3,5-dibenzhydrylidene-2-phenyl-[1,4,2]dioxaphospholane

Guidance literature:: phenylphosphine; diphenyl ketene; In pentane; at 20 ℃; for 18h;

With sodium hydroxide; In pentane; at 20 ℃; for 18h;
DOI:10.1002/ejic.200500454