2-Thiazolamine, N-cyclohexyl-4,5-dihydro-, monohydrochloride

Base Information

Chemical Name:2-Thiazolamine, N-cyclohexyl-4,5-dihydro-, monohydrochloride
CAS No.:80672-59-9
Molecular Formula:C9H16N2S.ClH
Molecular Weight:220.766
Hs Code.:

Synonyms:

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Chemical Property of 2-Thiazolamine, N-cyclohexyl-4,5-dihydro-, monohydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Thiazolamine, N-cyclohexyl-4,5-dihydro-, monohydrochloride

There total 10 articles about 2-Thiazolamine, N-cyclohexyl-4,5-dihydro-, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33024-70-3
1-cyclohexyl-3-(2-fluoroethyl)thiourea

: 80672-59-9
chlorhydrate de N-(thiazolin-2 yl-2) cyclohexylamine

Guidance literature:: Multi-step reaction with 4 steps

1: aq. HCl, sodium nitrite / CH₂Cl₂ / 2 h / -10 - -5 °C

2: 25 percent / potassium phosphate buffer (pH_7.2) / 12 h / 37 °C / decomposition by var. pH

3: 21 percent / diethyl ether / 3 h / 0 °C

4: 3 h / Ambient temperature

With hydrogenchloride; potassium phosphate buffer; sodium nitrite; In diethyl ether; dichloromethane;
DOI:10.1021/jo00170a006

Reference yield:

: 84081-66-3
3-cyclohexyl-1-(2-methoxyethyl)thiourea

: 80672-59-9
chlorhydrate de N-(thiazolin-2 yl-2) cyclohexylamine

Guidance literature:: Multi-step reaction with 4 steps

1: aq. HCl, sodium nitrite / CH₂Cl₂ / 2 h / -10 - -5 °C

2: 43 percent Chromat_. / potassium phosphate buffer (pH_7.2) / 12 h / 37 °C

3: 21 percent / diethyl ether / 3 h / 0 °C

4: 3 h / Ambient temperature

With hydrogenchloride; potassium phosphate buffer; sodium nitrite; In diethyl ether; dichloromethane;
DOI:10.1021/jo00170a006

Reference yield:

: 81467-07-4
N-cyclohexyl-N'-(2-hydroxyethyl)thiourea

: 80672-59-9
chlorhydrate de N-(thiazolin-2 yl-2) cyclohexylamine

Guidance literature:: Multi-step reaction with 4 steps

1: aq. sodium nitrite / CH₂Cl₂ / 2 h / -10 - -5 °C

2: 35 percent Chromat_. / potassium phosphate buffer (pH_7.2) / 12 h / 37 °C

3: 21 percent / diethyl ether / 3 h / 0 °C

4: 3 h / Ambient temperature

With potassium phosphate buffer; sodium nitrite; In diethyl ether; dichloromethane;
DOI:10.1021/jo00170a006