Benzenamine, N-[(5-methyl-2-thienyl)methylene]-

Base Information

Chemical Name:Benzenamine, N-[(5-methyl-2-thienyl)methylene]-
CAS No.:80833-74-5
Molecular Formula:C12H11NS
Molecular Weight:201.292
Hs Code.:
DSSTox Substance ID:DTXSID70359395
Nikkaji Number:J1.149.938D

Synonyms:80833-74-5;Benzenamine, N-[(5-methyl-2-thienyl)methylene]-;DTXSID70359395

Suppliers and Price of Benzenamine, N-[(5-methyl-2-thienyl)methylene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzenamine, N-[(5-methyl-2-thienyl)methylene]-

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:201.06122053
Heavy Atom Count:14
Complexity:197

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(S1)C=NC2=CC=CC=C2

Technology Process of Benzenamine, N-[(5-methyl-2-thienyl)methylene]-

There total 1 articles about Benzenamine, N-[(5-methyl-2-thienyl)methylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 13679-70-4
5-methylthiophene-2-carboxaldehyde

: 62-53-3
aniline

: 80833-74-5
N-(5-methyl-2-thienylmethylidene)aniline

Guidance literature:: In water; at 20 ℃; for 2h;
DOI:10.1039/b102749m

Reference yield: 74.0%

: 110-62-3
pentanal

: 80833-74-5
N-(5-methyl-2-thienylmethylidene)aniline

: N-((5-methylthiophen-2-yl)methyl)-N-pentylaniline

Guidance literature:: With HSiPh₃; In methanol; at 40 ℃; for 16h;
DOI:10.1039/c8cc05437a

Reference yield: 57.0%

: 17084-13-8
potassium hexafluorophosphate

: 37366-09-9
dichloro(benzene)ruthenium(II) dimer

: 75-05-8,26809-02-9
acetonitrile

: 80833-74-5
N-(5-methyl-2-thienylmethylidene)aniline

: 1259895-12-9
(Ru(SC₄H(CH₃)CHNC₆H₅)(CH₃CN)4)⁽¹⁺⁾*PF₆^(1-)=(Ru(SC₄H(CH₃)CHNC₆H₅)(CH₃CN)4)PF₆

Guidance literature:: With sodium hydroxide; In acetonitrile; (Ar) to suspn. Ru complex, NaOH and KPF6 in MeCN was added to imine, stirred at 45°C for 48 h; soln. was evapd. in vacuo, residue was chromd. on alumina (1-3 % CH2Cl2 in MeOH), soln. was concd. in vacuo, Et2O was added, ppt. was washed with Et2O; elem. anal.;
DOI:10.1021/ic101946n