Benzenepropanamide, a-amino-, (S)-, mono(trifluoroacetate)

Base Information

Chemical Name:Benzenepropanamide, a-amino-, (S)-, mono(trifluoroacetate)
CAS No.:81092-89-9
Molecular Formula:C9H12N2O.C2HF3O2
Molecular Weight:278.231
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepropanamide, a-amino-, (S)-, mono(trifluoroacetate)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenepropanamide, a-amino-, (S)-, mono(trifluoroacetate)

There total 4 articles about Benzenepropanamide, a-amino-, (S)-, mono(trifluoroacetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 81092-89-9
L-phenylalanine amide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N

2: 72.7 percent / 28percent NH₄OH, Et₃N / dimethylformamide / 6 °C

3: anisole

With ammonium hydroxide; methoxybenzene; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.46.452

Reference yield:

: 67729-36-6,60398-40-5
Boc-Phe-O-COO-isoBu

: 81092-89-9
L-phenylalanine amide trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 72.7 percent / 28percent NH₄OH, Et₃N / dimethylformamide / 6 °C

2: anisole

With ammonium hydroxide; methoxybenzene; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.46.452

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 81092-89-9
L-phenylalanine amide trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: isobutyl chloroformate; NH₄OH; Et₃N / dimethylformamide / 2 h / 20 °C

2: 1 h / 20 °C

With ammonium hydroxide; triethylamine; isobutyl chloroformate; In N,N-dimethyl-formamide;
DOI:10.1016/S0014-827X(00)00099-9