N-(4-CHLOROPHENYL)GLUTARIMIDE

Base Information

Chemical Name:N-(4-CHLOROPHENYL)GLUTARIMIDE
CAS No.:81305-70-6
Molecular Formula:C11H10ClNO2
Molecular Weight:223.659
Hs Code.:
Mol file:81305-70-6.mol

Synonyms:1-(4-Chloro-phenyl)-piperidine-2,6-dione;

Suppliers and Price of N-(4-CHLOROPHENYL)GLUTARIMIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N-(4-CHLOROPHENYL)GLUTARIMIDE Aldrich
1ea
$ 144.00

Total 3 raw suppliers

Chemical Property of N-(4-CHLOROPHENYL)GLUTARIMIDE

Chemical Property:

Boiling Point:455.1±28.0 °C(Predicted)
PKA:-1.25±0.20(Predicted)
PSA：37.38000
Density:1.342±0.06 g/cm3(Predicted)
LogP:2.44850

Purity/Quality:: N-(4-CHLOROPHENYL)GLUTARIMIDE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(4-CHLOROPHENYL)GLUTARIMIDE

There total 6 articles about N-(4-CHLOROPHENYL)GLUTARIMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 110-94-1
1,5-pentanedioic acid

: 106-47-8
4-chloro-aniline

: 81305-70-6
1-(4-chlorophenyl)piperidine-2,6-dione

Guidance literature:: 1,5-pentanedioic acid; With thionyl chloride; for 0.5h; Reflux;

4-chloro-aniline; In benzene; Reflux;

Reference yield: 55.0%

: 108-55-4
glutaric anhydride,

: 100-00-5
4-chlorobenzonitrile

: 81305-70-6
1-(4-chlorophenyl)piperidine-2,6-dione

Guidance literature:: 4-chlorobenzonitrile; With trichlorosilane; triethylamine; In acetonitrile; at 0 - 25 ℃; for 1h;

glutaric anhydride,; In acetonitrile; for 24h; chemoselective reaction;
DOI:10.1039/c9ra10758d