n-Hydroxy-4-methyl-n-phenylbenzamide

Base Information

Chemical Name:n-Hydroxy-4-methyl-n-phenylbenzamide
CAS No.:17120-16-0
Molecular Formula:C14H13 N O2
Molecular Weight:227.263
Hs Code.:
NSC Number:130257
DSSTox Substance ID:DTXSID90299421
Nikkaji Number:J582.813I
Wikidata:Q82041823
Mol file:17120-16-0.mol

Synonyms:n-hydroxy-4-methyl-n-phenylbenzamide;17120-16-0;NSC130257;DTXSID90299421;4-methyl-N-phenylbenzohydroxamic acid;NSC-130257

Suppliers and Price of n-Hydroxy-4-methyl-n-phenylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of n-Hydroxy-4-methyl-n-phenylbenzamide

Chemical Property:

Vapor Pressure:5.74E-07mmHg at 25°C
Boiling Point:395.6°Cat760mmHg
Flash Point:193°C
Density:1.234g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:227.094628657
Heavy Atom Count:17
Complexity:253

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)N(C2=CC=CC=C2)O

Technology Process of n-Hydroxy-4-methyl-n-phenylbenzamide

There total 5 articles about n-Hydroxy-4-methyl-n-phenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 874-60-2
4-methyl-benzoyl chloride

: 100-65-2
N-Phenylhydroxylamine

: 17120-16-0
N-phenyl-p-methylbenzohydroxamic acid

Guidance literature:: With sodium hydrogencarbonate; In water; at 0 - 5 ℃; for 2h;
DOI:10.1134/S0036023611110192

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 586-96-9
Nitrosobenzene

: 17120-16-0
N-phenyl-p-methylbenzohydroxamic acid

Guidance literature:: With 2-pentafluorophenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; N,N,N,N,-tetramethylethylenediamine; In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1002/asia.201300938

Reference yield:

: 98-95-3,26969-40-4
nitrobenzene

: 17120-16-0
N-phenyl-p-methylbenzohydroxamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; ammonium chloride / H₂O

2: NaHCO₃ / diethyl ether

With ammonium chloride; sodium hydrogencarbonate; zinc; In diethyl ether; water; 1: Reduction / 2: Acylation;