8-(Benzenesulfonyl)-8-methyl-1,4-dioxaspiro[4.5]dec-6-ene

Base Information

Chemical Name:8-(Benzenesulfonyl)-8-methyl-1,4-dioxaspiro[4.5]dec-6-ene
CAS No.:81841-91-0
Molecular Formula:C15H18O4S
Molecular Weight:294.372
Hs Code.:
DSSTox Substance ID:DTXSID10528508

Synonyms:8-(benzenesulfonyl)-8-methyl-1,4-dioxaspiro[4.5]dec-6-ene;81841-91-0;DTXSID10528508;8-methyl-1,4-dioxaspiro[4.5]dec-6-en-8-yl phenyl sulfone;8-methyl-8-(phenylsulfonyl)-1,4-dioxaspiro[4.5]dec-6-ene

Suppliers and Price of 8-(Benzenesulfonyl)-8-methyl-1,4-dioxaspiro[4.5]dec-6-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 8-(Benzenesulfonyl)-8-methyl-1,4-dioxaspiro[4.5]dec-6-ene

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:294.09258022
Heavy Atom Count:20
Complexity:479

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CCC2(C=C1)OCCO2)S(=O)(=O)C3=CC=CC=C3

Technology Process of 8-(Benzenesulfonyl)-8-methyl-1,4-dioxaspiro[4.5]dec-6-ene

There total 1 articles about 8-(Benzenesulfonyl)-8-methyl-1,4-dioxaspiro[4.5]dec-6-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 81841-89-6
4,4-(ethylenedioxy)-1-(phenylsulfonyl)cyclohexene

: 74-88-4
methyl iodide

: 81841-91-0
8-Benzenesulfonyl-8-methyl-1,4-dioxa-spiro[4.5]dec-6-ene

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)86766-0

Reference yield: 94.0%

: 81841-91-0
8-Benzenesulfonyl-8-methyl-1,4-dioxa-spiro[4.5]dec-6-ene

: 81842-30-0
4-methyl-4-(phenylsulfonyl)cyclohex-2-enone

Guidance literature:: With pyridinium p-toluenesulfonate; In acetone; for 3h; Heating;
DOI:10.1021/jo00173a040

Reference yield:

: 81841-91-0
8-Benzenesulfonyl-8-methyl-1,4-dioxa-spiro[4.5]dec-6-ene

: 5259-65-4
4-methyl-3-cyclohexen-1-one

Guidance literature:: With disodium hydrogenphosphate; sodium amalgam; toluene-4-sulfonic acid; Yield given. Multistep reaction; 1.) methanol, 2.5 h, 2.) ethanol, water, 20.5 h, reflux;
DOI:10.1021/jo00173a040