8-Benzyl-1,4-dioxaspiro[4.5]dec-7-ene

Base Information

Chemical Name:8-Benzyl-1,4-dioxaspiro[4.5]dec-7-ene
CAS No.:81842-02-6
Molecular Formula:C₁₅H₁₈O₂
Molecular Weight:230.307
Hs Code.:
DSSTox Substance ID:DTXSID10528528
Wikidata:Q82398235

Synonyms:8-Benzyl-1,4-dioxaspiro[4.5]dec-7-ene;81842-02-6;SCHEMBL13325881;DTXSID10528528

Suppliers and Price of 8-Benzyl-1,4-dioxaspiro[4.5]dec-7-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 8-Benzyl-1,4-dioxaspiro[4.5]dec-7-ene

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:230.130679813
Heavy Atom Count:17
Complexity:283

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2(CC=C1CC3=CC=CC=C3)OCCO2

Technology Process of 8-Benzyl-1,4-dioxaspiro[4.5]dec-7-ene

There total 3 articles about 8-Benzyl-1,4-dioxaspiro[4.5]dec-7-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 81842-02-6
8-Benzyl-1,4-dioxa-spiro[4.5]dec-7-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaH / dimethylformamide

2: 6 percent Na-Hg, Na₂HPO₄ / methanol / 0.5 h / Ambient temperature

With disodium hydrogenphosphate; sodium amalgam; sodium hydride; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)86766-0

Reference yield:

: 81841-89-6
4,4-(ethylenedioxy)-1-(phenylsulfonyl)cyclohexene

: 81842-02-6
8-Benzyl-1,4-dioxa-spiro[4.5]dec-7-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaH / dimethylformamide

2: 6 percent Na-Hg, Na₂HPO₄ / methanol / 0.5 h / Ambient temperature

With disodium hydrogenphosphate; sodium amalgam; sodium hydride; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)86766-0

Reference yield:

: 81841-94-3
6,6-(ethylenedioxy)-3-benzyl-3-(phenylsulfonyl)cyclohexene

: 81842-11-7
8-Benzyl-1,4-dioxa-spiro[4.5]dec-6-ene

: 81842-02-6
8-Benzyl-1,4-dioxa-spiro[4.5]dec-7-ene

Guidance literature:: With disodium hydrogenphosphate; sodium amalgam; In methanol; for 0.5h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1016/S0040-4039(00)86766-0