Ethyl 5-[1-(benzenesulfonyl)-4-oxocyclohex-2-EN-1-YL]pentanoate

Base Information

Chemical Name:Ethyl 5-[1-(benzenesulfonyl)-4-oxocyclohex-2-EN-1-YL]pentanoate
CAS No.:81842-38-8
Molecular Formula:C19H24O5S
Molecular Weight:364.463
Hs Code.:
DSSTox Substance ID:DTXSID00528517

Synonyms:81842-38-8;ETHYL 5-[1-(BENZENESULFONYL)-4-OXOCYCLOHEX-2-EN-1-YL]PENTANOATE;DTXSID00528517

Suppliers and Price of Ethyl 5-[1-(benzenesulfonyl)-4-oxocyclohex-2-EN-1-YL]pentanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Ethyl 5-[1-(benzenesulfonyl)-4-oxocyclohex-2-EN-1-YL]pentanoate

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:9
Exact Mass:364.13444504
Heavy Atom Count:25
Complexity:596

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)CCCCC1(CCC(=O)C=C1)S(=O)(=O)C2=CC=CC=C2

Technology Process of Ethyl 5-[1-(benzenesulfonyl)-4-oxocyclohex-2-EN-1-YL]pentanoate

There total 4 articles about Ethyl 5-[1-(benzenesulfonyl)-4-oxocyclohex-2-EN-1-YL]pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 81841-99-8
6,6-(ethylenedioxy)-3-(4-carbethoxybutyl)-3-(phenylsulfonyl)cyclohexene

: 81842-38-8
5-(1-Benzenesulfonyl-4-oxo-cyclohex-2-enyl)-pentanoic acid ethyl ester

Guidance literature:: With water; pyridinium p-toluenesulfonate; In acetone; for 2h; Heating;
DOI:10.1021/jo00173a040

Reference yield:

: 41302-32-3
ethyl 5-iodopentanoate

: 81842-38-8
5-(1-Benzenesulfonyl-4-oxo-cyclohex-2-enyl)-pentanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF

2: 80 percent / PPTS, H₂O / acetone / 2 h / Heating

With water; pyridinium p-toluenesulfonate; sodium hydride; In acetone;
DOI:10.1021/jo00173a040

Reference yield:

: 5535-48-8
PVS

: 81842-38-8
5-(1-Benzenesulfonyl-4-oxo-cyclohex-2-enyl)-pentanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) p-toluenesulfonic acid / 1.) benzene, reflux, 28 h, 2.) benzene, reflux, 23 h

2: 1.) NaH / 1.) DMF

3: 80 percent / PPTS, H₂O / acetone / 2 h / Heating

With water; pyridinium p-toluenesulfonate; sodium hydride; toluene-4-sulfonic acid; In acetone;
DOI:10.1021/jo00173a040