Hydrazinecarboxylic acid, 2-(4-methylbenzoyl)-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Hydrazinecarboxylic acid, 2-(4-methylbenzoyl)-, 1,1-dimethylethyl ester
CAS No.:820209-69-6
Molecular Formula:C13H18N2O3
Molecular Weight:250.298
Hs Code.:
DSSTox Substance ID:DTXSID90514565
Wikidata:Q82374957

Synonyms:tert-Butyl 2-(4-methylbenzoyl)hydrazine-1-carboxylate;820209-69-6;tert-butyl N-[(4-methylbenzoyl)amino]carbamate;N'-[(tert-butoxy)carbonyl]-4-methylbenzohydrazide;SCHEMBL17172491;DTXSID90514565;AKOS040766422;LS-12540;tert-butyl 2-(4-methylbenzoyl)hydrazinecarboxylate

Suppliers and Price of Hydrazinecarboxylic acid, 2-(4-methylbenzoyl)-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Hydrazinecarboxylic acid, 2-(4-methylbenzoyl)-, 1,1-dimethylethyl ester

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:250.13174244
Heavy Atom Count:18
Complexity:302

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)NNC(=O)OC(C)(C)C

Technology Process of Hydrazinecarboxylic acid, 2-(4-methylbenzoyl)-, 1,1-dimethylethyl ester

There total 4 articles about Hydrazinecarboxylic acid, 2-(4-methylbenzoyl)-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 870-46-2
t-butoxycarbonylhydrazine

: 624-31-7
4-tolyl iodide

: 820209-69-6
N-(4-methyl)benzoyl-N'-tertbutoxycarbonylhydrazine

Guidance literature:: With air; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium diacetate; In tetrahydrofuran; at 110 ℃; for 0.116667h; microwave irradiation;
DOI:10.1055/s-2004-832837

Reference yield:

: 99-94-5
p-Toluic acid

: 820209-69-6
N-(4-methyl)benzoyl-N'-tertbutoxycarbonylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 2 h / Heating

2: Et₃N / CH₂Cl₂ / 2 h

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jm00362a018