Phosphine, [(phenylborylene)bis(methylene)]bis[bis(1,1-dimethylethyl)-

Base Information

Chemical Name:Phosphine, [(phenylborylene)bis(methylene)]bis[bis(1,1-dimethylethyl)-
CAS No.:820219-05-4
Molecular Formula:C24H45BP2
Molecular Weight:406.38
Hs Code.:
DSSTox Substance ID:DTXSID80478541
Nikkaji Number:J2.130.466B

Synonyms:820219-05-4;Phosphine, [(phenylborylene)bis(methylene)]bis[bis(1,1-dimethylethyl)-;DTXSID80478541

Suppliers and Price of Phosphine, [(phenylborylene)bis(methylene)]bis[bis(1,1-dimethylethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Phosphine, [(phenylborylene)bis(methylene)]bis[bis(1,1-dimethylethyl)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:9
Exact Mass:406.3089556
Heavy Atom Count:27
Complexity:377

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B(CP(C(C)(C)C)C(C)(C)C)(CP(C(C)(C)C)C(C)(C)C)C1=CC=CC=C1

Technology Process of Phosphine, [(phenylborylene)bis(methylene)]bis[bis(1,1-dimethylethyl)-

There total 1 articles about Phosphine, [(phenylborylene)bis(methylene)]bis[bis(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.9%

: 873-51-8
phenylborondichloride

: 64065-07-2
(lithiomethyl)bis(tert-butyl)phosphane

: 820219-05-4
PhB(CH₂P((t)Bu)2)2

Guidance literature:: In diethyl ether; at -78 - 20 ℃; for 1h;
DOI:10.1021/ja0604358

Reference yield: 97.2%

: 820219-05-4
PhB(CH₂P((t)Bu)2)2

: copper(l) chloride

: 820219-12-3
[PhB(CH₂P(t)Bu₂)2CuCl]

Guidance literature:: In tetrahydrofuran; 1 equiv. of solid B-compd. and CuCl were combined in THF, stirring for 1h; soln. was filtered, volatiles were removed in vac., elem. anal.;
DOI:10.1016/j.poly.2004.08.008