5-Methylcyclohex-1-ene-1-carbaldehyde

Base Information

Chemical Name:5-Methylcyclohex-1-ene-1-carbaldehyde
CAS No.:82297-57-2
Molecular Formula:C8H12O
Molecular Weight:124.183
Hs Code.:
DSSTox Substance ID:DTXSID80512919
Nikkaji Number:J3.369.836D

Synonyms:82297-57-2;5-Methylcyclohex-1-ene-1-carbaldehyde;SCHEMBL1783414;DTXSID80512919

Suppliers and Price of 5-Methylcyclohex-1-ene-1-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 5-Methylcyclohex-1-ene-1-carbaldehyde

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:124.088815002
Heavy Atom Count:9
Complexity:136

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCC=C(C1)C=O

Technology Process of 5-Methylcyclohex-1-ene-1-carbaldehyde

There total 4 articles about 5-Methylcyclohex-1-ene-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: (2-Bromo-5-methyl-cyclohex-1-enyl)-methanol

: 82297-57-2
5R-methyl-cyclohexenecarboxaldehyde

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In benzene; for 8h; Heating;
DOI:10.1016/0040-4020(96)00715-6

Reference yield:

: 2-bromo-5-methylcyclohex-1-enecarbaldehyde

: 82297-57-2
5R-methyl-cyclohexenecarboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / NaBH₄ / methanol / -20 °C

2: 57 percent / Pd(OAc)2, PPh₃, K₂CO₃ / benzene / 8 h / Heating

With palladium diacetate; sodium tetrahydroborate; potassium carbonate; triphenylphosphine; In methanol; benzene;
DOI:10.1016/0040-4020(96)00715-6

Reference yield:

: 6134-75-4
5-methyl-2-oxocyclohexanecarboxylic acid ethyl ester

: 82297-57-2
5R-methyl-cyclohexenecarboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: pTsOH / benzene / 4 h / Heating

2: 51 percent / LAH / diethyl ether / 0 deg C, then RT, 2 h

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In diethyl ether; benzene;
DOI:10.1016/0040-4020(82)80183-X