2-Cyclopropene-1-carboxylic acid, 1-phenyl-

Base Information

Chemical Name:2-Cyclopropene-1-carboxylic acid, 1-phenyl-
CAS No.:824425-20-9
Molecular Formula:C10H8O2
Molecular Weight:160.172
Hs Code.:
DSSTox Substance ID:DTXSID90462572
Nikkaji Number:J2.141.932J

Synonyms:2-Cyclopropene-1-carboxylic acid, 1-phenyl-;824425-20-9;DTXSID90462572

Suppliers and Price of 2-Cyclopropene-1-carboxylic acid, 1-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-Cyclopropene-1-carboxylic acid, 1-phenyl-

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:160.052429494
Heavy Atom Count:12
Complexity:218

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2(C=C2)C(=O)O

Technology Process of 2-Cyclopropene-1-carboxylic acid, 1-phenyl-

There total 3 articles about 2-Cyclopropene-1-carboxylic acid, 1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 699005-11-3
1-phenyl-2-trimethylsilylcycloprop-2-ene carboxylic acid methyl ester

: 824425-20-9
1-phenylcycloprop-2-ene-1-carboxylic acid

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃;
DOI:10.1021/ol047837+

Reference yield:

: 101-41-7
benzeneacetic acid methyl ester

: 824425-20-9
1-phenylcycloprop-2-ene-1-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; 4-acetamidobenzenesulfonyl azide / acetonitrile / 20 °C / Cooling with ice

2: dirhodium tetraacetate / 10 h / 20 °C / Inert atmosphere

3: potassium hydroxide / methanol; water / 20 °C / Cooling with ice

With dirhodium tetraacetate; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium hydroxide; In methanol; water; acetonitrile;
DOI:10.1002/adsc.202000701

Reference yield:

: 22979-35-7
Methyl phenyldiazoacetate

: 824425-20-9
1-phenylcycloprop-2-ene-1-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dirhodium tetraacetate / 10 h / 20 °C / Inert atmosphere

2: potassium hydroxide / methanol; water / 20 °C / Cooling with ice

With dirhodium tetraacetate; potassium hydroxide; In methanol; water;
DOI:10.1002/adsc.202000701